GCMS scan report for Method 508, April 2002

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‘ Data File : C: \MSDCHEM\ 1 \DATA\ 020419\08271.D Vial: 9 Acq On : 19 Apr 2002 4:00 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Heptane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 3.13 0.29 ug/1 374840 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane 100 C7H16 000142-82-5 80 2 Heptane 100 C7H16 000142-82-5 72 3 Heptane 100 C7H16 000142-82-5 53 4 Heptane 100 C7H16 000142-82-5 50 Abundance Scan 8 (3.126 min): 08271 .D (-3) (-) m/z 43.15 100.00% 43

57 5000 71

P . 100 84 3.20 3.30 3.40 3.50 3.60 49 1 ----- 0- i ■ ■ ■ ■ i ■ 1 ■ ■ i ■ ■ ■ ■ i ' ' ■ 11 1 47''I 1’1" I ' ' TTT m/z 57.10 55.28% n/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #109303: Heptane 43

5000 29 57 71 7 .) T—n 11! 3.20 3.30 3.40 3.50 3.60 m/ z 71.10 49.48% 100

1‘111‘un/n.k —37 +5114 1 15 65 . 77 85 0- ITT■ 1 ■ I1 ‘ I4B41* 1I.I m/z-> 0 10 20 30 40 50 60 70 80 90 100 Abundance #109668: Heptane 43 __ i t CIIT 1^ I I J I I I I I I t ■ 1 I / 3.20 3.30 3.40 3.50 3.60

5000 57 m/z 41.10 48.82% 71 29

0- ■ ■ i ■ ■ ■ ■ i ■ ■ ■ • । 22■ |1 1 i ■ 1 37440 +5114+63 +7785.91 199— n/z-> 0 10 20 30 50 60 ( 70 80 90 100 Abundance #109598: Heptane 48 3.20 3.30 3.40 3.50 3.60 m/z 56.10 31.73% 5000 57 29 71

m/z—> 0 ' 0 +4374 +511 60 ' i ' ‘ 1 ' i ■ 10 20 30 40 50 63 11 70 80 85 90 100 - 100 PMA-MA--AA- 3.20 3.30 3.40 3.50 3.60

08271.D SCANAPR0902.M Mon Apr 22 15:45:03 2002 Page 14

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