GCMS analysis results for sample AE09571, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9570.D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 15 1H-Imidazole-4-methanol, 5-. Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 32.64 1.57 ug/L 2729440 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1H-Imidazole-4-methanol, 5-methyl- 112 C5H8N2O 029636-87-1 9 2 Cyclohexene, 3,5-dimethyl- 110 C8H14 000823-17-69 3 5-Hexen-l-one, 1-(lH-imidazol-4-... 192 C11H16N20 069393-41-5. 9 4 Cyclohexanemethanol, .alpha.-(2-... 168 C11H20O 031569-55-8 9 Abundance Scan 5031 (32.639 min): 9570.D (-5030) (-) m/z 83.10 100.00% 57 83 95 111 welanwpt"t 150 5000 134 178 . 209 231 261 43 194 163 32.40 32,60 32.80 33.00 01 i ' 1 . i . III --------------------- m/z 95.10 89.84% 1il 1 i '' 1 'I 1 miz-> :20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #41480:1 H-lmidazole-4-methanol, 5-methyl- MMwArMAwvwp 95

5000 112 42 32.40 32.60 32.80 33.00 54 83 m/z 57.10 73.81% III 68

n/z-> 0! :20 ... 40lr al,60 d, 80 100 120 140 160 180 200 220 240 260 118 ■ i - ■ ■ ■ i ■ ■ ■ - i ■ ■ * > i ■ .M-P"yMhuMqpMhhna Abundance #118150: Cyclohexene, 3,5-dimethyl- 95 32.40 32.60 32.80 33.00 67 5000 m/z 111.10 60.50%| 41 55 110 27 i 81 I, ill ill ______________________________________ 0 111 pph 4 ' ' T 1 • 1 r I ‘ ‘ ■ 1 1 1 ■ ■ 1 1 1 * 1 1 1 ' 1 ■ ■ I 1 1 1 ■ I 1 ’ • ■ I 1 ■ ’ 1 1 1 ' T0B n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #41469:5-Hexen-1 -one, 1 -(1 H-imidazol-4-yl)-4,4-dimethyl- 95 32,40 32.60 32.80 33.00 m/z 108.00 51.92% 110 5000 41

55 69

81 123 136 149 183 I77 192 \ pMh+“ MyaMHMwe 0 —274. , oe । , 4—ll + — •nlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 32.40 32.60 32.80 33.00

9570.D 050102.M Mon May 13 11:46:49 2002 Page 21

NYC-WTC_000023048