GCMS calibration data for TCLP method, May 2002

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000022930–000022937

Folder label: “GCMS X 5/8/02 A 5/10/02”

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Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY0 3 02\9 5 6 8.D Vial: 42 Acq On 5 May 2002 8:11 am Operator: Sample GC/MS SCAN 4/23 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:34 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration < DataAcq Meth : GCMS0501 ’

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 505317 40.00 ug/1 -0.03 10) Naphthalene-d8 15.83 136 1849505 40.00 ug/1 -0.03 17) Acenaphthene-dl0 21.13 164 1003869 40.00 ug/1 -0.02 30) Phenanthrene-dl0 25.58 188 1408946 40.00 ug/1 -0.02 38) Chrysene-dl2 33.64 240 911524 40.00 ug/1 -0.03 44) Perylene-dl2 37.86 264 591940 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.28 209 19269 3.94 ug/L -0.02 Spiked Amount 10.000 Recovery = 39.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 11.46 93 661 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Is opho rone 14.54 82 730 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 573 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.41 162 223 N.D. 20) Dimethylphthalate 20.48 163 898 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 20.66 152 324 N.D. 2 3) Acenaphthene 21.22 153 385 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.62 149 3986 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.75 166 500 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.64 178 2283 N.D.

(#) = qualifier out of range (m) = manual integration 9568.D GCMS0501.M Tue May 07 14:34:26 2002 Page 1

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

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