Volatile organic compounds blank analysis results, March 22, 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02mar22\0322R5A.D Vial: 5 Acq On . 22 Mar 2002 2:21 pm Operator: 201-wb Sample : ref 5. no gases Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 22 15:00 2002 Quant Results File: HP031802.RES Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri Mar 22 09:11:28 2002 Response via : Initial Calibration DataAcq Meth : HP031802

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.09 114 1005536 5.00 ug/L 0.04 24) CHLOROBENZENE-D5 21.74 117 910758 5.00 ug/L 0.04 52) 1,4-DICHLOROBENZENE-D4 26.93 152 500719 5.00 ug/L 0.05 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 468975 5.66 ug/L 0.04 Spiked Amount 5.000 Recovery = 113.20% 3) 4-BROMOFLUOROBENZENE 24.33 174 394687 4.86 ug/L 0.04 Spiked Amount : 5.000 Recovery = 97.20% 25) TOLUENE-D8 18.44 98 1168695 5.30 ug/L 0.04 Spiked Amount 5.000 Recovery = 106.00% Target Compounds Qvalue 12) ACETONE 8.24 43 118964 18.10 ug/L 96 13) 1,1-DICHLOROETHENE 8.58 61 263905 4.39 ug/L 98 14) METHYLENE CHLORIDE 9.59 49 232444 4.35 ug/L 98 15) METHYL TERT BUTYL ETHER 9.89 73 225416 4.18 ug/L 98 16) TRANS-1,2-DICHLOROETHENE 10.25 61 265602 4.40 ug/L 98 17) 1,1-DICHLOROETHANE 11.15 63 308058 4.45 ug/L 95 18) 2-BUTANONE (MEK) 11.99 43 111509 15.08 ug/L 99 19) 2,2-DICHLOROPROPANE 12.36 77 267003 4.91 ug/L 95 20) CIS-1,2-DICHLOROETHENE 12.46 96 181366 4.46 ug/L 99 21) CHLOROFORM 12.80 83 365513 4.89 ug/L 100 22) BROMOCHLOROMETHANE 13.18 49 132964 4.28 ug/L 95 23) 1,2-DICHLOROETHANE 14.52 62 257553 4.98 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.69 97 297236 5.78 ug/L 99 27) 1,1-DICHLOROPROPENE 14.01 75 234363 4.95 ug/L 99 28) CARBON TETRACHLORIDE 14.27 117 265464 5.99 ug/L 99 29) BENZENE 14.61 78 569320 4.83 ug/L 97 30) TRICHLOROETHENE 15.89 95 190033 5.16 ug/L 98 31) 1,2-DICHLOROPROPANE 16.24 63 141515 4.60 ug/L 95 32) DIBROMOMETHANE 16.92 174 91820 5.27 ug/L 98 33) BROMODICHLOROMETHANE 16.77 83 240732 5.17 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 48036 3.91 ug/L 94 35) METHYL ISO-BUTYL KETONE 17.33 58 92952 17.70 ug/L 98 36) CIS-1,3-DICHLOROPROPENE 17.86 75 207493 4.65 ug/L 98 37) TOLUENE 18.63 91 628367 4.98 ug/L 98 38) TRANS-1,3-DICHLOROPROPENE 18.90 75 155248 4.72 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.27 97 104341 5.01 ug/L 97 40) TETRACHLOROETHENE 20.07 166 205555 5.50 ug/L 94 41) 1,3-DICHLOROPROPANE 19.82 76 179773 4.68 ug/L 95 42) DIBROMOCHLOROMETHANE 20.50 129 137787 5.12 ug/L 92 43) 1,2-DIBROMOETHANE 20.96 107 101083 4.76 ug/L 100 44) CHLOROBENZENE 21.83 112 426725 5.02 ug/L 100 45) 1,1,1,2-TETRACHLOROETHANE 21.88 131 162146 5.40 ug/L 95 46) 2-HEXANONE 19.17 43 163106 16.78 ug/L 98 47) ETHYLBENZENE 21.88 91 753367 5.13 ug/L 99 48) P & M-XYLENE 22.03 106 513138 10.25 ug/L 94 49) O-XYLENE 23.00 91 594049 5.15 ug/L 96 50) STYRENE 23.07 104 382768 5.00 ug/L 99 51) 1,1,2,2-TETRACHLOROETHANE 24.09 83 95877 4.55 ug/L 100 53) BROMOFORM 23.92 173 68132 5.09 ug/L 98 54) ISOPROPYLBENZENE 23.73 105 674596 5.05 ug/L 100 55) 1,2,3-TRICHLOROPROPANE 24.42 110 33777 4.66 ug/L 99 (#) = qualifier out of range (m) = manual integration 0322R5A.D HP031802.M Fri Mar 22 15:00:43 2002 Page 1

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