Volatile organic compounds results, Mar 14 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02mar14\06052D.D Vial: 10 Acq On : 14 Mar 2002 5:26 pm Operator: 201-wb Sample : nyc; dup Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 1-(Propenylthio)prop-l-ene Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.75 0.03 ug/L 17104 1,4-DIFLUOROBENZENE 15.10 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O21 006843-45-4 3 3 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 2 4 2,4,5-Trioxoimidazolidine 114 C3H2N203>000120-89-8 2 Abundance Scan 692 (15.750 min): 06052D.D (-) m/z 114.15 100.00% 1 4 8000

6000

4000 15.40 15.60 15.80 16.00 50 88 m/z 49.95 25.37% i ■ ' • • i ‘ ■ i ■ ■ ■ ■ I ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i ‘ * i ■ ■ ■ ■ i ■ m/z--> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2940:1-(Propenylthio)prop-1-ene 1 4 41 99

5000 15.40 15.60 15.80 16.00 m/z 88.00 24.75% 73 85 47 59 144**114*** ‘ 1 ■ । * * • * । * ‘ * > । ■ i ' ■ ■ ■ i ■ • ■ ■ i ■ ■ ■ ■ i ■' TT-p-r /z--> 20 30 40 50 60 80 70 90 100 110 120 Abundance #64088: 2,4-Imidazolidinedione, 3-methyl- 1 4

‘ i ■ 1 ■ ‘ i ‘ ■ ■ ' i •' 1 1 i 1 15.40 15.60 15.80 16.00 58 5000

86 42 71 1**’’I’2**1’’’’I* ■ i ■ ■ • ■ i ■ ■ ■ ■ i ■ -n/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64087:3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 29 58

5000 114

.... 1141...... i ■ ■ •11 ‘ ■ ■ ■ I' ' ■ ■ i ■ ■ 68 86 i ‘ ‘ ‘ ■ i ‘ 1 ' ' i ‘ ' 1 ' l ' ■ ‘ ‘ i ' ■ ' ■ i ■ 14114 m/z-> 20 30 40 50 60 70 80 90 100 110 120

06052D.D HP022702.M Thu Mar 14 18:05:17 2002 Page 1

NYC-WTC_000021790