Volatile organic compounds results, Mar 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02MAR13\5896A.D Vial: 11 Acq On : 13 Mar 2002 7:07 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 1-(Propenylthio)prop-l-ene Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 15.80 0.03 ug/L 25857 1,4-DIFLUOROBENZENE 15.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O21 006843-45-4 3 3 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 2 4 2,4,5-Trioxoimidazolidine 114 C3H2N2031 000120-89-8 2 Abundance Scan 695 (15.801 min): 5896A.D (-) m/z 114.15 100.00% 1 4

5000

63 88 L 15.40 15.60 15.80 16.00 16.20 44 i ■ ■ ■ ■ i ■ ' ■ ■ i ' ■ ■ ■ i ‘ ■ i ■ ■ ■ ' i ■ ■ 1 1 i ' ■ m/z 63.05 23.75% /z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2940:1-(Propenylthio)prop-1-ene 1 4 41 99

5000 T -p-mr-p-r 15.40 15.60 15.80 16.00 16.20 m/z 88.00 20.92% 73 85 A 47 59

m/z--> i 4 1 k 1 I * ’ • ’ i ‘ 20 30 40 4 50 60 I . TIit 70 80 90 100 ■ i ■11 ■ i ■ ■ ■ ■ ! ' ■ ■ ■ i 110 •'

120 Abundance #64088:2,4-Imidazolidinedione, 3-methyl- 1 4 I 15.40 15.60 15.80 16.00 16.20 58 m/z 43.95 0.60% 5000

86 MWWMMMWN ...... 42... 71 ■i ■ ■ ■ ■ i'■■■i■■ ' i ■ ‘ ■ ■ i ‘ ‘ ' I ‘ m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #64087:3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 29 15.40 15.60 15.80 16.00 16.20 58

5000 114

... I I ■ ‘ 1 ‘ I ‘ 41 rt ■ ■ I 1 1 68 SI444*I’FISIAI’’’I4 86 m/z-> 20 30 40 50 60 70 80 90 100 110 120

5896A.D HP022702.M Thu Mar 14 11:27:22 2002 Page 1

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