Volatile organic compounds results, Mar 14 2002

NYC 9/11 Public Portal Document Library.Search Compound Report Data File : C:\HPCHEM\1\DATA\02mar14\06051.D Vial: 8 Acg On : 14 Mar 2002 3:59 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C: \HPCHEM\1\METHODS\HP022702 .M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 1-(Propenylthio)prop-l-ene Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.75 0.03 ug/L 15109 1,4-DIFLUOROBENZENE 15.08

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1-(Propenylthio)prop-1-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2! 006843-45-4 3 3 2,4,5-Trioxoimidazolidine 114 C3H2N2031 000120-89-8 2 4 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H204 _________002892-51-5 2 Abundance Scan 691 (15.749 mln): 06051 .D (-) m/z 114.15 100.00% 1 14

5000 63 88 ■ । l ■ > • ■ l ■ 50 1 I " " I' 15.40 15.60 15.80 16.00 44 m/z 88.10 31.08% • • i ' ■ ■ m/z-> 40 50 60 70 80 90 100 110 120 Abundance #2940: 1-(Propenylthio)prop-1-ene 1 4 41 99

5000 15.40 15.60 15.80 16.00 m/z 63.05 28.75% 59 73 85 47 ■ ■ i1 ■ 41 i ' ■ ■ ■ i ■ ■ ■ ■ i • ' i 1 • ' ■ i ■ ' T-r-j-r-r m/z-> 40 50 60 70 80 90 100 ’110 120 Abundance #64088:2,4-Imidazolidinedione, 3-methyl- 1 14

15.40 15.60 15.80 16.00 58 m/z 50.25 24.60% 5000

86

42 71 n-T-r-rr-r-r-T-r-r-p ■ i 1 1 1 1 I 1 ‘ i 1 ■ m/z-> 40 50 60 70 80 90 100 110 120 Abundance #2824:2,4,5-Trioxoimidazolidine ‘I T TIt 43 15.40 15.60 15.80 16.00 m/z 44.00 9.23%

5000 86 114 MMMAW 70

m/z--> — 40 --54- 50 —PPPPP 60 70 80 90 1 i 1 1 ■ ■ i • ■ ■ ■ i ■ 100 110 120 15.40 15.60 15.80 16.00

06051.D HP022702.M Thu Mar 14 16:38:33 2002 Page 1

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