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Volatile organic compounds analysis results, March 25, 2002

Machine-extracted title · confidence 95%

Laboratory report detailing analytical results for volatile organic compounds in sample AE06981 collected on March 25, 2002.

NYC-WTC_000022304–000022414

Folder label: “524 3/25/02

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Scanned page image, NYC-WTC_000022356
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\02MAR25\6986.D Vial: 10 Acq On : 25 Mar 2002 9:12 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP031802.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1- 1-(Propenylthio)prop-l-ene Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.70 0.03 ug/L 19355 1,4-DIFLUOROBENZENE 15.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-(Propenylthio)prop-1-ene 114 C6H10S. 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2: 006843-45-4 3 3 2,4,5-Trioxoimidazolidine 114 C3H2N203, 000120-89-8 2 4 3-Cyclobutene-1,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 2 Abundance Scan 689 (15.698 min): 6986.D (-) m/z 114.15 100.00% 1 4

5000

50 63 88 ' 1 I ' 1 1 1 i ' ' ' ' I ' 1 1 ' 1 1 1 15.40 15.60 15.80 16.00 44 m/ z 63.05 25.11% 1 1 i 1 1 i ■ 1 ' ■ i 1 ' ■ 1 i 1 1 1 i 1 1 A m/z--> S 40 50 60 70 80 90 100 110 120 Abundance #2940: 1 -(Propenylthio)prop-I -ene 1 4 41 99

5000- 15.40 15.60 15.80 16.00 m/ z 87.90 22.53% 59 73 85 (

m/z-> • ■ t ’ ■ 40 +— 11I.. 47 I 1 11 1 1 50 I 60 70 80 1 i ' 1 ' ' I ' ' ' ' i 1 90 100 110 ■ ■ 120 i ■ ■

Abundance #64088: 2,4-Imidazolidinedione, 3-methyl- 1 4 - 15.40 15.60 15.80 16.00 58 m/z 49.85 22.47% 5000-

86

42 i ■ i ■ ■ ■ ■ 71 i ■ ■ ■ ■ i ■ • ' i ' 1 ‘ 1 i 1 ' i ' 1 1 ' i 1 1 1 ' i ' 1 1 I ’ 1 m/z-> 40 50 60 70 80 90 100 110 120 Abundance #2824: 2,4,5-Trioxoimidazolidine 43 ‘ (‘‘‘‘I’ 1 ■ i ' • ‘ ' i ' 1 15.40 15.60 15.80 16.00 m/z 43.95 4.06%

5000 - 86 114 MAMM 70 54..... li...... ■ 1 1 1 ■ 1 i ' 1 ' ' i ' 1 1 r I ' 1 1 1 i ■ ■ ' i r ■ ' ‘ i ' 1 ' ■ i ■ 1 1 1 1 1 118 m/z-> 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00

6986.D HP031802.M Tue Mar 26 08:26:18 2002 Page 1

NYC-WTC_000022356

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NYC-WTC_000022356Source: NYC Law Department, mirrored locally

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