Volatile organic compounds results, Mar 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\O2MAR13\5702A.D Vial: 9 Acq On : 13 Mar 2002 5:40 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-(Propenylthio)prop-l-ene Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

15.80 0.03 ug/L 28497 1,4-DIFLUOROBENZENE 15.14

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 2 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O21 006843-45-4 3 3 3-Cyclobutene-l,2-dione, 3,4-dihydr 114 C4H204 002892-51-5 2 4 2,4,5-Trioxoimidazolidine 114 C3H2N203i • 000120-89-8 2 Abundance Scan 695 (15.801 min): 5702A.D (-) m/z 114.05 100.00% 1 4

5000 63 88 15.40 15.60 15.80 16.00 16.20 ................................. 50........ |................... m/z 63.05 27.25% ‘ ■ i ■'

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #2940:1-(Propenylthio)prop-1-ene 1 4 41 99

5000 15.40 15.60 15.80 16.00 16.20 m/z 88.10 24.89% 59 73 85 ■ ■ i' ■ • ■ i ■ “ ‘ i ‘ ‘1 ■ i ‘ ■1 ■ i • ‘‘ i''' ■ i " i1" TITTu 'I' ■1 ■ i ■' TT-p-r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #64088:2,4-lmidazolldinedione, 3-methyl- 1 4 i ■ ■ ■1 i ■ ' ■ ■ i ■ ■ i ■ ■ ■ ' i ‘ 1

15.40 15.60 15.80 16.00 16.20 58 m/z 50.05 16.03% 5000

86 42 71 i ■ ■' ■ i'' ■ ■ i ■' ‘ i ■ •'' i ■ ■ • ■ i ■ • ■ i 1' i1 ■ ‘11 ■ “ ‘ i ‘ ‘1 ■ i ■11' i'1 11

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #2826: 3-Cyclobutene-1,2-dione, 3,4-dihydroxy- 23 58 15.40 15.60 15.80 16.00 16.20

5000 114

86 17 40 m/z-> 10 20 —P 68 ’ i111 • i■■■■ i ■■ 30 40 50 60 70 80 90 100 110 120 .""211112111 • ■ i * ■

5702A.D HP022702.M Thu Mar 14 11:24:14 2002 Page 1

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