Volatile organic compounds results, Mar 14 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02mar14\06050.D Vial: 7 Acq On : 14 Mar 2002 2:47 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Ethanamine, N-methyl-N-nitroso Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

15.75 0.03 ug/L 24848 1,4-DIFLUOROBENZENE 15.08

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanamine, N-methyl-N-nitroso- 88 C3H8N20 010595-95-6 3 2 1,2-Hydraz inedicarboxaldehyde 88 C2H4N2021 000628-36-4 3 3 Sulfide, allyl methyl 88 C4H8S 010152-76-8 3 4 1-(Propenylthio)prop-l-ene 114 C6H10S ________ 000000-00-0 3 Abundance Scan 692 (15.749 min): 06050.D (-) m/z 114.15 100.00% 1 4

5000

63 88 4a isieo is'so is'oo . 44 m/z 63.05 24.49% 11 ■ ■ ‘ • i ■ ■ ■ ■ i ■ ■ ■ • i' ■ ■ ■ i • ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ 1 ■ ■ ‘ ' i '' ' ' i ■

m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62895: Ethanamine, N-methyl-N-nitroso- 42 88

5000 15.40 15.60 15.80 16.00 m/z 88.10 21.48% 56 73 m/z-> MiTT’TT 1100011—0001)3 ■ i'' ■ ‘ i' ■ ■11 ■ ■' ■ i 10 20 30 40 50 60 70 80 90 100 110 120 11 ‘ I ‘ 11 '

Abundance #62891: 1,2-Hydrazinedicarboxaldehyde 31

15.40 15.60 15.80 16.00 5000 95 5.23

16 60 88 WWM 45

/z-> |... II... h ■ i ■ ■1 ■ i ‘ ■

10 20 30 40 50 60 70 80 90 100 110 120 1 11 • ■ ■ ■ 1 •' i ■ ■ ‘ ■ i ‘ ‘ ‘ i ■ ■ ' ‘ i ■ ‘

Abundance #62927: Sulfide, allyl methyl 41 15'46 15.60 15.80 16.00 T 73 88 5000

61

m/z-> ■ i ‘‘ ‘ i • ■ ■111 ■ ■' i ■ 10 20 30 40 484 50 60 70 80 90 ■' i ■ ■ ■ ■ i ■ ■ '' i ‘1 100 110 120

06050.D HP022702.M Thu Mar 14 15:26:52 2002 Page 1

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