Volatile organic compounds results, Mar 13 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02MAR13\5701A.D Vial: 7 Acq On : 13 Mar 2002 4:13 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Ethanamine, N-methyl-N-nitroso Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.77 0.03 ug/L 21883 1,4-DIFLUOROBENZENE 15.10 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanamine, N-methyl-N-nitroso- 88 C3H8N20 010595-95-6 3 2 Sulfide, allyl methyl 88 C4H8S 010152-76-8 3 3 1,2-Hydraz inedicarboxaldehyde 88 C2H4N202 000628-36-4 3 4 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N202 006843-45-4 3 Abundance Scan 693 (15.766 min): 5701A.D (-) m/z 114.05 100.00% 1 4

5000

63 88 1....... ..... I 15.40 15.60 15.80 16.00 44 TT-rm m/z 88.10 26.18% m/z-> 10 ■ i ■ ■ ■ ■ i111 ‘ i ■ ■ ‘ ■ i ■ ■ ■ ‘ i ■ ■ ‘ ■ i ■ ■ ■ ■ i •' •11 • ■ 20 30 40 50 60 70 80 90 100 I ■ ‘ ' I ‘ ' I ' 110 120 N Abundance #62895: Ethanamine, N-methyl-N-nitroso- 42 88

5000 ■ i ■ ■ ' ■ i1 ' ' ■ i ‘ ‘ ‘ i ■ 15.40 15.60 15.80 16.00 m/z 62.95 23.70 56 73 m/z--> hp — ■ i ■ ■ ■ ■ l ' ‘ 10 20 30 40 50 60 70 ' i ■ ■ ‘ ■ i 80 90 100 110 120 i ‘ ■ ■ ■ i ■ ‘111 ■ ■ ■ ‘ i ‘1

Abundance #62927: Sulfide, allyl methyl 41 T-pn-n-p-r ■ ' I ‘ ‘ ' I ' 73 88 15.40 15.60 15.80 16.00 5000 m/z 44.00 6.14%

61 WMWwWyMA ............................... ' i'''' i ■ ■ ‘ ■ i ‘' i ■ mmpmm rn/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62891:1,2-Hydrazinedicarboxaldehyde • i ■ ■ > ■ ITT । i । । । । । . 31 15.40 15.60 15.80 16.00

5000 88 60 16 45

m/z-> ,1 ... 1111 10 20 30 40 50 60 1 1 i ' ‘' i ‘ ‘ 70 80 .i.... । *1.. ।।. 90 100 110 120

5701A.D HP022702.M Thu Mar 14 11:22:08 2002 Page 1

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