Volatile organic compounds results, Mar 7 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\02mar07\5164.D Vial: 12 Acq On 7 Mar 2002 7:24 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 Ethanamine, N-methyl-N-nitroso Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 15.72 0.03 ug/L 25033 1,4-DIFLUOROBENZENE 15.07 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanamine, N-methyl-N-nitroso- 88 C3H8N20 010595-95-6 3 2 Sulfide, allyl methyl 88 C4H8S 010152-76-8 3 3 1,2-Hydraz inedicarboxaldehyde 88 C2H4N202’ 000628-36-4 3 4 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O2!006843-45-4 3 Abundance Scan 690 (15.715 mln): 5164.D (-) m/z 114.05 100.00% 1 14

5000

63 88 A.... ... ........ 15.40 15.60 15.80 16.00 44 ■ I ■ ■ ■ ■ I ■ ■ ■ ■ i ■ ■ ■ ' i • ■ ‘' i ‘ ■ i ‘ I ' i • • ■ 1 i ■' I ' ■ ■ ■ i 1 ' ■ ■ 1 1 m/z 88.10 29.06% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62895: Ethanamine, N-methyl-N-nitroso- 42 88

5000 15.40 15.60 15.80 16.00 m/z 63.05 19.38% 56

/z-> ■ I 1 ■ ■ ■ I ■ ‘ 10 20 ‘ i ‘ 30 ‘ ■ i LL 40 50 60 70 80 90 73 I ■ ■ i ■ • ‘ ■ i ■ ■ *’l ' ‘ ‘ ‘ I ‘ ‘ ‘ ' I ■ ■ ‘ 1 I'1 100 110 120 Abundance #62927: Sulfide, allyl methyl 41 T T 73 88 15.40 15.60 15.80 16.00 5000 m/z 43.95 6.88%

61 MWyHhv m/z-> 10 ■ I'1■11 ■ ■ 1 ■ i ■ ■ ■ ■ i' 20 414 30 40 50 60 70 80 90 100 110 120 mmmmmp

Abundance #62891: 1,2-Hydrazinedicarboxaldehyde 31 TTF T T T 15.40 15.60 15.80 16.00

5000 60 88

16 I 45......... ■ i ■ ■1 ■ i • ■ 1′144414* i ■ ■ ■ ■ i ■11 ■ i ■1 ■' 111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120

5164.D HP022702.M Thu Mar 07 20:03:25 2002 Page 1

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