VOC analysis results, sample AE03944, Feb 20 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB20\03950.D Vial: 15 Acq On : 20 Feb 2002 7:48 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 20, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 4 Ethanamine, N-methyl-N-nitroso Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 15.80 0.04 ug/L 48891 1,4-DIFLUOROBENZENE 15.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethanamine, N-methyl-N-nitroso- 88 C3H8N20 010595-95-6 3 2 1,4-Dioxane 88 C4H802 000123-91-1 3 3 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 4 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N2O21 006843-45-4 3 Abundance Scan 694 (15,800 min): 03950.D (-) m/z 114.05 100.00% 1'4

5000 63 88

m/z-> 10 ..........43.50 11........... '' I ‘ ‘ ‘' I' ‘■ I' ‘ ‘' I' ‘ ‘ ‘ 1 ‘ 20 30 40 50 '11'11 • i ■ ■ ■ ■ i ■ ■ 60 70 80 90 i ■ ■ ■ ■ i' ■' ‘ i ■ 100 110 120 ■ ■ i •1 15.40 15.60 15.80 16.00 16.20 m/z 63.05 29.29%

Abundance #62895: Ethanamine, N-methyl-N-nitroso- 42 88

5000 15.40 15.60 15.80 16.00 16.20 m/z 88.10 22.84% 56 73 m/z- II TTTnr '' 10 "2o " "3o " 4o' 50 60 70 80 90 100 110 120 1 T-pt-T-rp-T

Abundance #794: 1,4-Dioxane 29 88 58 15.40 15.60 15.80 16.00 16.20 m/z 49.95 13.53% 5000 15

m/z-> H 10 —rr 20 30 40 50 60 70 80 90 100 110 120 I ■ ' ‘' I ■ ‘1 • 111 i ■' • ■ i ■ ■ ■ ■ i • ■ ■ ■ i ■ ■

Abundance #2940:1-(Propenytthlo)prop-1-ene 11 1 4 15.40 15.60 15.80 16.00 16.20 41 99 m/z 57.05 12.68% A 5000

m/z—> • ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । ■' ■ ■ । 10 20 30 40 ... 59.. 73.75, ■1 ■ । ■ ■ ■ ■ । ■'1' ।' । ■ p ■ • ■ । 50 60 70 80 90 ■ I ""I1' T-rpr-r 100 110 120 15.40 15.60 15.80 16.00 16.20

03950.D HP021702.M Fri Feb 22 09:35:33 2002 Page 4

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