VOC analysis results, sample AE03934, Feb 27 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\02FEB27\0227C10A.D Vial: 17 Acq On : 27 Feb 2002 9:54 pm Operator: Sample : cal 10 Inst : 210 Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: GAS5.P Quant Time: Feb 28 8:08 2002 Quant Results File: HP021102.RES

Quant Method : C:\HPCHEM\1\METHODS\HP021102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Thu Feb 28 08:07:11 2002 Response via : Initial Calibration DataAcq Meth : HP021102

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.58 114 1095447 5.00 ug/L 0.00 21) CHLOROBENZENE-D5 23.34 82 580645 5.00 ug/L 0.00 49) 1,4-DICHLOROBENZENE -D4 29.39 152 493093 5.00 ug/L 0.00

System Monitoring Compounds 2) 1,2-Dichloroethane-d4 14.63 65 255319 5.49 ug/L 0.00 Spiked Amount 5.000 Recovery = 109.80% 22) Toluene-d8 19.49 98 1397478 4.76 ug/L 0.00 Spiked Amount 5.000 Recovery = 95.20% 50) 4-Bromofluorobenzene 26.39 95 516081 5.01 ug/L 0.00 Spiked Amount 5.000 Recovery = 100.20%

Target Compounds Qvalue 3) DICHLORODIFLUOROMETHANE 4.22 85 764482 10.60 ug/L 99 4) CHLOROMETHANE 4.83 50 813602 13.14 ug/L 98 5) VINYL CHLORIDE 4.89 62 1069064 13.88 ug/L 99 6) BROMOMETHANE 5.75 96 512447 10.23 ug/L 96 7) CHLOROETHANE 5.88 64 676745 13.95 ug/L 98 8) TRICHLOROFLUOROMETHANE 6.40 101 796014m 11.04 ug/L 9) ACETONE 8.04 43 14698m 11.85 ug/L 10) 1,1-DICHLOROETHENE 7.80 61 933851 9.16 ug/L 93 11) METHYLENE CHLORIDE 8.98 49 927696 9.75 ug/L 92 12) METHYL TERT BUTYL ETHER 9.29 73 1229658 9.56 ug/L 99 13) TRANS-1,2-DICHLOROETHENE 9.73 61 1063271 10.22 ug/L 93 14) 1,1-DICHLOROETHANE 10.82 63 1369630 10.84 ug/L 98 15) 2-BUTANONE (MEK) 12.25 43 72312 15.69 ug/L 93 16) 2,2-DICHLOROPROPANE 12.26 77 948508 10.27 ug/L 99 17) CIS-1,2-DICHLOROETHENE 12.40 61 1087440 10.99 ug/L 95 18) CHLOROFORM 12.79 83 1316079 10.87 ug/L 98 19) BROMOCHLOROMETHANE 13.25 49 493544 10.74 ug/L 91 20) 1,2-DICHLOROETHANE 16.91 62 553441 10.62 ug/L 100 23) 1,1,1-TRICHLOROETHANE 13.82 97 1040511 10.50 ug/L 99 24) 1,1-DICHLOROPROPENE 14.24 75 1059063 10.07 ug/L 98 25) CARBON TETRACHLORIDE 14.50 117 746088 10.17 ug/L 99 26) BENZENE 14.93 77 816492 9.45 ug/L 100 27) TRICHLOROETHENE 16.47 95 809290 9.91 ug/L 100 28) 1,2-DICHLOROPROPANE 16.91 63 784445 9.98 ug/L 99 29) DIBROMOMETHANE 17.68 174 238520 9.51 ug/L 96 30) BROMODICHLOROMETHANE 17.50 83 772093 9.67 ug/L 99 31) 2-CHLOROETHYL VINYL ETHER 19.69 63 286298 10.77 ug/L 95

(#) = qualifier out of range (m) = manual integration 0227C10A.D HP021102.M Thu Feb 28 08:08:41 2002 Page 1

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