VOC analysis results, sample AE03944, Feb 20 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB20\03946.D Vial: 12 Acq On : 20 Feb 2002 5:39 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 20, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Silane, methyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 7.87 0.45 ug/L 428331 1,4-DIFLUOROBENZENE 15.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Silane, methyl- 46 CH6Si 000992-94-9 7 2 1-Butanamine, N, 3-dimethyl- 101 C6H15N 004104-44-3 5 3 1-Pentanamine, N-methyl- 101 C6H15N 025419-06-1 5 4 lH-Pyrrole, 1-methyl- 81 C5H7N ______ 000096-54-8 5 Abundance Scan 229 (7.867 min): 03946.D (-) m/z 81.00 100.00% 81

5000 45 61 101 7.60 7.80 8.00 8.20

m/z-> mm "■I1-1"' 10 20 30 40 50 60 70 80 ■ i > • • > । • ■ ■ ■ । 1 90 100 110 m/z 45.05 32.18%

Abundance #46: Silane, methyl- 44

5000 N.. WVVY 7.60 7.80 8.00 8.20 29 m/z 83.00 30.68% 15 . I. —1 • i < ■ • ■ । ■ ■ • ■ | i • i • • ■ * 11 • * ■ i • • ■ • i • ‘ • i ■ ■ • • i ■ * i • । * m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1658: 1-Butanamine, N,3-dimethyl- 44 • ■ • ■ i ■ • • • i ■ ■ • ■ i ■ ■ • • i • ■ ■' 7.60 7.80 8.00 8.20 5000 m/z 60.95 23.96%

101 30 58 —mPPP ■ ■ l ■ ■ ■ 11 ■ ■ ■ ■ i72 86 I ■ ■ ■ ' i ■ ■ ' ■ i ■ ■ • ■ I' ■ 1 ' i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1646: 1-Pentanamine, N-methyl- 44 7.60 7.80 8.00 8.20 m/z 101.00 8.87%

5000

30 101 86 | mPmpuT .. I ... 11|■ ’1111*111111111818 58 70 ■ ■ i ■ ■ ■ i ■ ■ • ■ i ■ ■ m/z--> 10 20 30 40 50 60 70 80 90 100 110 7.60 7.80 8.00 8.20

03946.D HP022702.M Mon Mar 04 17:11:59 2002 Page 1

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