SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\02FEB04 \01937F. D Vial: 13 Acq On : 4 Feb 2002 7:09 pm Operator: 201-wb Sample : nyc fb Inst : GC/MS Ins. Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butanoic acid, methyl ester Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

16.59 0.06 ug/L 50877 1,4-DIFLUOROBENZENE 15.15

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 74 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0 5 3 1-Pentanamine 87 C5H13N 000110-58-7 4 4 Formic acid, ethyl ester 74 C3H602 000109-94-4 4 Abundance Scan 730 (16.593 min): 01937F.D (-) m/z 43.05 100.00% 43 8000 74 6000

4000 59 87 16.20 16.40 16.60 16.80 17.00 ■ ■ i ' ■ ■ ■ i ‘ 1 1 ■ i ' i ■ ■ ■ i 1 ■ • ■ i ■ ■ ■ ' i ■ ■ ■ ■ i ■ * m/z 74.05 67.80% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63493: Butanoic acid, methyl ester 43 74

5000 ■ i ‘ ' 1 i 1 ' ‘ ■ i ■ ■ 1 ■ i ■ ■

27 16.20 16.40 16.60 16.80 17.00 15 59 87 m/z 41.05 52.44% ......... .............. | 33 102 — ■ i 1 1 ■ ■ 1 1 ' i ■ ■ ■ ■ i ' ■ • ■ i 1 ■ ■ • i niz-> 10 20 30 40 50 60 _________________ 70 80 90 100 110 Abundance #752:3-Pyrrolidinol 43 / l 16.20 16.40 16.60 16.80 17.00 5000 m/z 71.05 45.91% 87 57 68

niz-> 10 20 30 40 1 ‘ I 1 ■‘'■''I ' 50 60 70 I..... 80 1 Hu । । । । i । । । i ■ । 90 100 110 Abundance #776: 1-Pentanamine 33 16.20 16.40 16.60 16.80 17.00 m/ z 38.95 27.71%

5000

m/z—> — 10 20 30 4. . ............ ..... n 40 50 60 70 80 90 100 110 16.20 16.40 16.60 16.80 17.00

01937F.D HP013102.M Tue Feb 05 09:37:20 2002 Page 5

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