SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02FEB04\01937F.D Vial: 13 Acq On : 4 Feb 2002 7:09 pm Operator: 201-wb Sample : nyc fb Inst : GC/MS Ins Mise 2002 : February 4, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Hexane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

15.93 0.03 ug/L 24436 1,4-DIFLUOROBENZENE 15.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane 86 C6H14 000110-54-3 5 2 Azetidine, 1-nitroso- 86 C3H6N20 015216-10-1 4 3 3-Pentanone 86 C5H10O 000096-22-0 4 4 2-Penten-l-ol, (E)- 86 C5H10O 001576-96-1 3 Abundance Scan 692 (15.931 min): 01937F.D (-) m/z 57.05 100.00% 57

5000 ' ■ i ' ■ ■ • i * * i * 1 • * । 86 15.60 15.80 16.00 16.20 3942 m/z 86.10 20.61% ■' i' ■'' i “ “ i' " ' i' " ‘ i " " I “ ‘' i " '' i' 1 ■ i1 ■ “ i1 ■ ■ ■ i " " i " " i “ ■' i ' i'11 ■ i ■ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62874: Hexane 43 57

5000 15.60 15.80 16.00 16.20 86 m/ z 39.05 18.57% 39 '11 “ 1' 11' rii ma H 53, 71 11" " i “ 1 ■ I* ■ i' ■ ‘' i''' • i ' ■ i ■ ■ ■ ■ i ■ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #646: Azetidine, 1-nitroso- 33 ________________ i’’114+I+’’*I ■ 1 i ■ ■ 15.60 15.80 16.00 16.20 41 m/z 41.95 17.15% 5000 86 44 55

38 52 - rri 11111 TT —H ■ ■ i ■ ■ • ■ i' niz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62848:3-Pentanone 29 57 15.60 15.80 16.00 16.20

5000

86 26 42 — TITr fIHTTT TTH i < । ■ ■ ■ ■ । ■ *1 * । ■11 ■ । ■1 ■ I *11 * । '"IFTTu i1 /z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

01937F.D HP013102.M Tue Feb 05 09:37:18 2002 Page 4

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