VOC analysis results, sample AE02089, Feb 7 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\0 2 febO 6\2 3 8 5F.D Vial: 14 Acq On 7 Feb 2002 4:04 am Operator: 201-wb '.7 Sample fb Inst : GC/MS Ins— Mise : Multiplr: 1.00 — MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) ~asdm

Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Hexane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

15.90 0.03 ug/L 41616 1,4-DIFLUOROBENZENE 15.13 enndn-

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane 86 C6H14 000110-54-3 5 2 Isocrotonic acid 86 C4H602 000503-64-0 5 3 3-Pentanone 86 C5H10O 000096-22-0 4 ■bn 4 Azetidine 57 C3H7N 000503-29-7 3 -is Abundance Scan 690 (15.896 min): 2385F.D (-) m/z 57.05 100.00% -== 57

5000

86 ■ ■ i 1 ■ 1 ■ i ‘ ■ i

..... 4033 ... "111-1TTT22317"T-1’-1-1"--IT ’ I’’ ’!’ 15.60 15.80 16.00 16.20 m/z 86.10 20.82% ■n/z-> 20253035 40 4550556065 70 75 80859095 Abundance #62874: Hexane 43 57

5000 n ... . 15.60 15.80 16.00 16.20 86 rn/z 43.05 13.05% 39 71 - - +753+ —— niz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #660: Isocrotonic acid 39 —15.60 AMAAm15.80 16.00 16.20 86 m/z 41.95 12.47% 5000 68 42 45 60

niz-> ■ ■ i " '' i ■1" i ■ ■ " i ■ 20 25 30 35 4 40 57 71 1111 ■ ■ I'1 ‘11'' TIIT —TT 45 50 55 60 65 70 75 80 85 ■ ■ i ■1111 ■ 90 95 Abundance #723:3-Pentanone II........ .................... ... ■ I 29 57 15.60 15.80 16.00 16.20 m/z 41.05 12.41%

5000

86 26 37 43 53 , 11 • >»• । • • • ■ । • i l • i ■ • > > ।> 11 +10 T-r-p-r ■ ■ i ■ ■ ■ ■ i1 " i' " ■ i ■" ■ i ■1 ■11 ■ " ‘ I ■ i ■ ■ ■ ■ 11 Th ITUt 1 1 n/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 15.60 15.80 16.00 16.20

2385F.D HP013102.M Thu Feb 07 04:44:49 2002 Page 3

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