VOC analysis results, sample AE02089, Feb 7 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02feb06\2385F.D Vial: 14 — Acq On 7 Feb 2002 4:04 am Operator: 201-wb — Sample fb Inst : GC/MS Ing— Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCS BY EPA METHOD'524 Library : C:\DATABASE\NBS75K.L ********************************************************************* •MM

Peak Number 4 Butanoic acid, methyl ester Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 16.56 0.06 ug/L 69750 1,4-DIFLUOROBENZENE 15.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual — 1 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 78 2 Azetidine, 1-methyl- 71 C4H9N 004923-79-9 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 3-Pyrrolidinol 87 C4H9NO 040499-83-0 5 Abundance Scan 728 (16.558 min): 2385F.D (-) m/z 43.05 100.00%

A 43 74

5000 A.... ‘I***I‘ 59 87 16.20 16.40 16.60 16.80 ....................... 36.1 II 1 ■ ■ i ■ ■ ■ • i ■ ■ ■ ■ i • ■ ■ ■ i 1 ■ i ' ■ ■ ■ i ■ ■ ' ■ i 1 m/z 74.05 75.19% n/z-> 10 20 30 40 50 60 70 80 ' 90 100’ 110 Abundance #63490: Butanoic acid, methyl ester 43 74 5000 27 16.20 16.40 16.60 16.80 ' ' ' ' 59 m/z 71.15 55.42% 87 37 ----------+ | 102 A ■ ■ i ■ ' ■ ■ i ■ ■ ■ ■ i ■ ■ ' ■ i ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ r '"' 1 ' r miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #246: Azetidine, 1-methyl- 33 42

16.20 16.40 16.60 16.80 ‘ ' 5000 56 m/z 41.05 46.56% 71

"n * I ' ' ■ i ' ■ ‘ ■ I1 ■ ■ ■ i ■ ■ ■ 1 i ■ ■ ■ • i ‘ ■ i niz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 33 16.20 16.40 16.60 16.80 ' ‘ ‘ ' m/z 39.15 31.72%

5000

15 41 • • । । * L ■ ■ 111 । ■ 55 70 87 T T T /z—> 10 20 30 40 50 60 70 80 90 100 110 16.20 16.40 16.60 16.80

2385F.D HP013102.M Thu Feb 07 04:44:50 2002 Page 4

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