VOC analysis results, sample AE03944, Feb 20 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB20\03946.D Vial: 12 Acq On : 20 Feb 2002 5:39 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 20, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 2 Silane, fluorotrimethyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.80 0.17 ug/L 164985 1,4-DIFLUOROBENZENE 15.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Silane, fluorotrimethyl- 92 C3H9FSi 000420-56-4 90 2 Acetamide, 2-fluoro- 77 C2H4FNO 000640-19-7 9 3 4,6-Heptadiyn-3-one 106 C7H60 029743-27-9 9 4 3,5-Hexadiyn-2-one 92 C6H40 ______ 031097-80-0 4 Abundance Scan 107 (5.803 min): 03946.D (-) m/z 77.10 100.00% 77

5000 47 ATMPP 5.40 5.60 5.80 6.00 6.20 ................... 1...... 3..... I... 92001301 ■ • i ■ ■ •11 ■ ■ • ‘ i ' ■ ■ ■ i ‘ * • * i *’’+1*’’I* m/z 46.95 27.59% n/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #956: Silane, fluorotrimethyl- 77

5000 5.40 5.60 5.80 6.00 6.20 47 m/z 48.95 18.71% 63 m/z-> 10 15 ■ ■ i ■ 1 ■ ' i ■ ■ 20 27 30 Xi I ■ ' • ' i ' ■ 40 50 -PP 1—PPmmr IT 92 60 70 80 90 100 110 Abundance #387: Acetamide, 2-fluoro- 44

77 5.40 5.60 5.80 6.00 6.20 5000 m/z 62.95 7.25%

33 ............... 60 * > i > • • > i • •..• • ] • • • > । i hotpt 1 i ‘ ■ i • ‘ ‘ ■ i ■ ■ ■ 1 I 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #2021:4,6-Heptadiyn-3-one i • ■ • * i ■ ■ ■ ’ i 1 11 " ‘' I " 77 5.40 5.60 5.80 6.00 6.20 m/z 78.10 7.21%

5000

29 49 57 63 pA i i 106 ''i 1 1' ‘ I ■ • ‘ ■ i ‘ ‘1 ■ i • • । • • • > i • ■ • ■ i ■ ■ i ■ ■ ‘ ■ i ' ■ ' ■ i ■ ■ ' ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 5.40 5.60 5.80 6.00 6.20

03946.D HP021702.M Fri Feb 22 09:29:53 2002 Page 2

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