VOC analysis results, sample AE02089, Feb 7 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\02feb06\2381.D Vial: 9 Acq On 6 Feb 2002 10:17 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCS BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Propanamine, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

9.93 0.03 ug/L 28907 1,4-DIFLUOROBENZENE 15.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual .-

1 1-Propanamine, 2-methyl- 73 C4H11N 000078-81-9 3 2 1 - But anamine 73 C4H11N 000109-73-9 3 3 DL-3,4-Dimethyl-3,4-hexanediol 146 C8H1802 032388-94-6 2 4 Methane, nitroso-_____________________ 45 CH3NO 000865-40-7 2 Abundance Scan 347 (9.926 min): 2381 .D (-) m/z 73.05 100.00% 73

5000 x<Ge 40 43 57

9.60 m/z 9.80 10.00 10.20 43.05 61.29% ‘ ’ I'1' ‘ I' ‘‘ 11 *' ‘"I ‘' I ‘ 1)88/4/213 “ i1" 11 ■ ■ ■ i ■ ■' ‘ i ■ ‘■ i ■' ' i ■ “ ■ i ■ ■ n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #62540:1 -Propanamine, 2-methyl- 30

5000 9.60 9.80 10.00 10.20 m/z 57.05 57.76% 27 43 46 55 58 ? ■ ■ i ■ ■ • ■ i " ■' i' ■'' i'1 ‘1 111—a0*p—u—mu*uW—tpmur /z-> 5 10 15 2025303540455055 60 65 70 75 80 Abundance #62539:1-Butanamine 33 ....................................... 9.60 9.80 10.00 10.20 ' ' ' 5000 m/z 41.15 53.97%

15 | ri । । | । । 111 11 । । | । H+ 27 37 41 44 56 73 H I I I I I H I I I I I I I I I I I I I I I I I I I 11 I I I I I 1 I I ■ I I I h I II '•I‘ 1 N, N

mz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #8865: DL-3,4-Dimethyl-3,4-hexanediol 43 9.60 9,80 10.00 10.20 ' ' m/z 45.15 36.28%

5000 73 55

/z—> 5 11111" i111' । ■ •'11 ■ ■ ■11" " i • ■ ■ ■ ।

10 15 20 25 30 35 40 1 I,.... .h,. 65.... 70tt 45 50 55 60 ' i' ■' ■ i'' 75 80 9.60 9.80 10.00 10.20 '

2381.D HP013102.M Wed Feb 06 22:57:26 2002 Page 1

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