VOC analysis results, sample AE03015, Feb 15 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02FEB15\03015D.D Vial: 20 Acq On : 15 Feb 2002 11:56 pm Operator: 201-wb Sample : nyc dup Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2,3-Dioxabicyclo [2.2.2]octane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

15.79 0.04 ug/L 36417 1,4-DIFLUOROBENZENE 15.13

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,3-Dioxabicyclo[2.2.2]octane 114 C6H10O2 000000-00-0 4 2 Urea, N,N-dimethyl- 88 C3H8N20 000598-94-7 4 3 Ethanedial , dioxime 88 C2H4N2021 000557-30-2 4 4 1,4-Butanediamine 88 C4H12N2 _______ 000110-60-1 3 Abundance Scan 683 (15.791 min): 03015D.D (-) m/z 114.15 100.00% 1 4

5000

63 88 50 15.40 15.60 15.80 16.00 16.20 ‘■■.-rm,!,,,, 40 I | i m/z 88.00 20.60% ■ ■ i1'1 ■ i' ■' ■ i' ■ ■ i' ■' ■ i ■ ■ ■ ■ i'

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #2867:2,3-Dioxabicyclo[2.2.2]octane 29

5000 57 81 i ■ ■ ■ 11' ' i ■ • ■ ■ i ■ ■ ■11 ■ ■ 114 15.40 15.60 15.80 16.00 16.20 44 m/z 62.95 19.98% 67 — ■ । । > 1| .,, ।।।. ■ ■ i ■1 ■ • i > > ■ ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62896: Urea, N,N-dimethyl- 44

15.40 15.60 15.80 16.00 16.20 5000 m/z 57.05 16.53% 88

15

m/z-> L ■ ■ i ■ . 56 72 । 30 + ' ■ i ■ ' ' • i ■ ■ ' ■ i ' ■ 1 ■ i ‘ ‘

10 20 30 40 50 60 70 80 90 100 110 120 ''i' ■ ■ ■ i ■ ■ ■ ■ i ■ ■' ■ i ■1

Abundance #783: Ethanedial, dioxime 44 i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ' ' i ■1 ■ ■ i ■ ■

15.40 15.60 15.80 16.00 16.20 16 m/z 50.05 13.47% 27 88 70 5000

53 ... ■ ■ i ■ ■ * i • ■ 111—0111’00177 ’i’t mmT i ■ ■ ' ■ i ■ i' ■ ■ ■ i '1 1 ' 11 ‘ m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00 16.20

03015D.D HP021302.M Mon Feb 18 15:22:56 2002 Page 1

NYC-WTC_000019882