VOC analysis results, sample AE03958, Feb 19 2002

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Data File : C:\HPCHEM\1\DATA\02FEB19\03956.D Vial: 3 Acq On : 19 Feb 2002 7:21 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 19, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Urea, N,N-dimethyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 15.75 0.03 ug/L 13345 1,4-DIFLUOROBENZENE 15.08 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Urea, N,N-dimethyl- 88 C3H8N20 000598-94-7 5 2 2,3-Dioxabicyclo[2.2.2]octane 114 C6H10O2 000000-00-0 4 3 2-Pentenoic acid, 4-methyl- 114 C6H10O2 010321-71-8 4 4 1,4-Butanediamine 88 C4H12N2 _________000110-60-1 3 Abundance Scan 692 (15.749 min): 03956.D (-) m/z 114.05 100.00% 1 4

8000

6000 T-p-r-n-p-r T-p-n-n-p 4000 15.40 15.60 15.80 16.00 63 88 m/z 88.00 23.94% * * 1 ■ ■ i ■ • ■ ■ i ■ • ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ‘ ‘ ■ i ■ ■ ■11 ■ /z-> 10 2030405060 70 8090 100 110 120 Abundance #62896: Urea, N,N-dimethyl- 44

5000 88 15.40 15.60 15.80 16.00 m/z 63.05 23.62% 15

m/z-> 4 ■ ■ i ■ + — 72 30 10 20 30 40 50 60 70 80 90 100 110 120 • * I ‘ ■OO 1 t ‘ t ■ ■ ■ ■ 11 ■ ■ ‘ I •

Abundance #2867:2,3-DioxabicycIo[2.2.2]octane 29 15.40 15.60 15.80 16.00 5000 81 57 114 44 67

m/z-> 10 ••j••>•। • 20 30 " i ■ 40 50 60 70 80 90 dam 4 ■ ‘ i ■ ■ ■ ■ i''' ■ i' 100 110 120 ■ ■ i ■'

Abundance #2882:2-Pentenoic acid, 4-methyl- 43

5000 59 69 99

m/z-> H 81 | ■ ■ i ■ ‘ ‘ ■ i' ■' ■ i ■' ■ ‘ i ‘ 10 20 30 40 50 60 70 80 90 100 110 120 rjT.t ’ । 1’ t * , । p ,nyn-

03956.D HP021702.M Mon Mar 04 10:41:19 2002 Page 1

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