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VOC analysis results, sample AE03384, Feb 17 2002

Machine-extracted title · confidence 95%

Laboratory results for volatile organic compounds in sample AE03384 analyzed on February 17, 2002.

NYC-WTC_000019981–000020025

Folder label: “524 2/17/02

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Scanned page image, NYC-WTC_000020025
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB17\03390.D Vial: 8 Acq On : 17 Feb 2002 8:10 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Urea, N,N-dimethyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 15.79 0.04 ug/L 56595 1,4-DIFLUOROBENZENE 15.13 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Urea, N,N-dimethyl- 88 C3H8N20 000598-94-7 5 2 Urea, ethyl- 88 C3H8N20 000625-52-5 4 3 2,3-Dioxabicyclo [2.2.2]octane 114 C6H10O2 000000-00-0 4 4 Ethanol, 2-(methylamino)- 75 C3H9NO ______ 000109-83-1 4 Abundance Scan 684 (15.792 min): 03390.D (-) m/z 114.05 100.00% 1 4

5000 63 88 h 15.40 15.60 15.80 16.00 16.20 Its

m/z-> 10 ... ..... 38.5° 20 30 40 50 60 70 80 90 • i»■ > > i ■ 75 • i • • I | । I i i । i i i i |-r-

100 110 120 m/z 63.05 26.78%

Abundance #62896: Urea, N,N-dimethyl- 44

5000 88 l ■' ■ ‘ i ■ ‘ ■ i T 15.40 15.60 15.80 16.00 16.20 m/z 88.10 24.73% 15

m/z-> Q 10 30 - ■ ■ । ■56 72 1 ■ । ■ ■ ■ ■ 11 ■ ■' i1'

20 30 40 50 60 70 80 90 100 110 120 i ■ ■ ■ ■ i ■ ■' ■ i ■ ■' ■ i ■1

Abundance #789: Urea, ethyl- 30 44 73 11 ■ ■1111 88 15.40 15.60 15.80 16.00 16.20 5000 m/z 56.95 14.30%

56

m/z-> 10 '11' 771 20 H 30 ' 40 50 60 70 80 90 100 110 120 i ■ ‘ ■ ■ i ■ ■ ■ ‘ i ‘ ■ ■ ■ i ‘1

Abundance #2867:2,3-Dioxabicyclo[2.2.2]octane 29 15.40 15.60 15.80 16.00 16.20 m/z 50.05 11.98%

5000 57 81 114 44 67 T-r-p-rr-rp-r TT-p- . . ...।.,.,!....|| l ■ ■ ■ ■ i ■1 i ■ ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 15.40 15.60 15.80 16.00 16.20

03390.D HP022702.M Fri Mar 01 16:47:41 2002 Page 1

NYC-WTC_000020025

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NYC-WTC_000020025Source: NYC Law Department, mirrored locally

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