VOC analysis results, sample AE03958, Feb 19 2002

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Data File : C:\HPCHEM\1\DATA\02FEB19\03957.D Vial: 4 Acq On : 19 Feb 2002 8:04 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 19, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2,3-Dioxabicyclo (2.2.2]octane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 15.73 0.03 ug/L 23841 1,4-DIFLUOROBENZENE 15.09 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2,3-Dioxabicyclo [2.2.2]octane 114 C6H10O2 000000-00-0 4 2 Urea, N,N-dimethyl- 88 C3H8N20 000598-94-7 4 3 Butane, 2-(ethenyloxy) -2-methyl- 114 C7H140 029281-39-8 3 4 3-Pentanone, 2,4-dimethyl- 114 C7H140 ______ 000565-80-0 3 Abundance Scan 691 (15.732 min): 03957.D (-) m/z 114.15 100.00% 1 4 8000

W.. 0.... 6000

4000 63 88 15.40 15.60 15.80 16.00 rrj-n m/z 63.05 33.04% ' • i ■' ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ‘ i ■ ■' ■ i ■ ■' ■ i ■ ■ ■' i ■ ■ ■' i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #2867:2,3-Dioxabicyclo[2.2.2]octane 29

5000 57 81 114 15.40 15.60 15.80 16.00 44 m/z 88.10 27.07% 67 m/z-> 10 ..... l... 20 30 "It 40 ... 1...

50 60 70 80 90 100 110 120 ■ ‘ i ■ ‘ ■ ■ i ■ ■1' i ■ ■ ■ i'1

Abundance #790: Urea, N,N-dimethyl- 44

88 15.40 15.60 15.80 16.00 5000 m/z 57.05 22.05%

15 30 ■ ■ i ■ ■ 1 • i ■ ‘ I ■ ' ■ ■ i' 56 ' • i ■ ■1 ■ i ■ ‘' J ‘ 72 ■ i ■' I ■' ■ ■ i ■ ■'' i ■ ■ ‘' i ‘ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #3032: Butane, 2-(ethenyloxy)-2-methyl- 43 15.40 15.60 15.80 16.00

5000

55 71 85 114 27

m/z--> mm I.'.... 1.... 99.... 1.... 10 20 30 40 50 60 70 80 90 100 110 120 i • ■ ■ • i * '

03957.D HP021702.M Mon Mar 04 10:42:51 2002 Page 1

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