VOC analysis results, sample AE03015, Feb 15 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02FEB15\0215C10A.D Vial: 18 Acq On : 15 Feb 2002 10:17 pm Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 17 12:54 2002 Quant Results File: HP021302.RES Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Sun Feb 17 12:54:35 2002 Response via : Initial Calibration DataAcq Meth : HP021302

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.11 114 1753368 5.00 ug/L 0.00 24) CHLOROBENZENE-D5 21.78 117 1660150 5.00 ug/L 0.02 52) 1,4-DICHLOROBENZENE-D4 26.95 152 789563 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 612139 4.59 ug/L 0.00 Spiked Amount 5.000 Recovery = 91.80% 3) 4-BROMOFLUOROBENZENE 24.36 174 607565 4.61 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.20% 25) TOLUENE-D8 18.47 98 2127108 5.17 ug/L 0.00 Spiked Amount 5.000 Recovery = 103.40% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.89 85 585361 9.48 ug/L 98 5) CHLOROMETHANE 5.51 50 579506 12.29 ug/L 100 6) VINYL CHLORIDE 5.62 62 308786 14.85 ug/L 99 7) BROMOMETHANE 6.60 94 345950 12.11 ug/L 98 8) CHLOROETHANE 6.75 64 334786 11.61 ug/L 95 9) TRICHLOROFLUOROMETHANE 7.30 101 689203 12.44 ug/L 99 12) ACETONE 8.27 43 86015 7.14 ug/L 97 13) 1,1-DICHLOROETHENE 8.62 61 794885 9.43 ug/L 98 14) METHYLENE CHLORIDE 9.63 49 858793 8.48 ug/L 94 15) METHYL TERT BUTYL ETHER 9.93 73 818370 7.31 ug/L 94 16) TRANS-1,2-DICHLOROETHENE 10.29 61 917775 8.51 ug/L 95 17) 1,1-DICHLOROETHANE 11.18 63 1059094 8.32 ug/L 97 18) 2-BUTANONE (MEK) 12.01 43 199764 7.15 ug/L 97 19) 2,2-DICHLOROPROPANE 12.40 77 698772 6.84 ug/L 98 20) CIS-1,2-DICHLOROETHENE 12.50 96 610034 8.38 ug/L 97 21) CHLOROFORM 12.83 83 1037392 8.11 ug/L 97 22) BROMOCHLOROMETHANE 13.22 49 524755 8.62 ug/L 99 23) 1,2-DICHLOROETHANE 14.56 62 667479 7.75 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.72 97 784729 8.47 ug/L 94 27) 1,1-DICHLOROPROPENE 14.05 75 820384 8.88 ug/L 98 28) CARBON TETRACHLORIDE 14.31 117 654641 8.70 ug/L 100 29) BENZENE 14.64 78 2154222 8.98 ug/L 100 30) TRICHLOROETHENE 15.93 95 629738 8.78 ug/L 93 31) 1,2-DICHLOROPROPANE 16.28 63 616583 9.10 ug/L 95 32) DIBROMOMETHANE 16.96 174 282294 8.77 ug/L 92 33) BROMODICHLOROMETHANE 16.80 83 721748 8.32 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.27 63 187493 7.48 ug/L 92 35) METHYL ISO-BUTYL KETONE 17.36 58 102576 8.26 ug/L 91 3 6) CIS-1,3-DICHLOROPROPENE 17.88 75 815204 8.52 ug/L 98 37) TOLUENE 18.65 91 2265375 9.04 ug/L 99 3 8) TRANS-1,3-DICHLOROPROPENE 18.92 75 570586 8.14 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.31 97 352609 8.68 ug/L 99 40) TETRACHLOROETHENE 20.09 166 637641 9.34 ug/L 98 41) 1,3-DICHLOROPROPANE 19.83 76 691440 8.69 ug/L 99 42) DIBROMOCHLOROMETHANE 20.53 129 410043 8.39 ug/L 97 43) 1,2-DIBROMOETHANE 20.98 107 358276 8.14 ug/L 98 44) CHLOROBENZENE 21.85 112 1475081 9.22 ug/L 94 45) 1,1,1,2-TETRACHLOROETHANE 21.90 131 486419 9.07 ug/L 97 46) 2-HEXANONE 19.20 43 263882 10.59 ug/L 99 47) ETHYLBENZENE 21.90 91 2623635 9.08 ug/L 97 48) P & M-XYLENE 22.06 106 1781054 18.07 ug/L 93 (#) = qualifier out of range (m) = manual integration 0215C10A.D HP021302.M Sun Feb 17 12:55:03 2002 Page 1

NYC-WTC_000019872