VOC analysis results, sample AE02575, Feb 8 2002

NYC 9/11 Public Portal Document Llorary aearen compound Report -i Data File C: \HPCHEM\ 1 \DATA\ 02feb08\2710.D Vial: 12 -f Acq On 9 Feb 2002 1:51 am Operator: 201-wb Sample nyc 524 Inst : GC/MS Ins 2 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP020502.M (RTE Integrator) — Title : VOCs BY EPA METHOD 524 - Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Azulene Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. - 32.78 0.06 ug/L 69384 1,4-DICHLOROBENZENE-D4 26.93 ait - Hit# of 5 Tentative ID MW MolForm CAS# Qual “ wifi l Azulene 128 C10H8 000275-51-4 83 llt 2 Naphthalene 128 C10H8 000091-20-3 83 -lt - 3 lH-Indene, 1-methylene- 128 C10H8 002471-84-3 83 k 4 [4.2.2]Propella-2,4,7,9-tetraene 128 C10H8 088090-34-0 40 Abundance 1660 (32,779 min): 2710.D (-) m/z 128.15 100.00% -di wa / 128

5000

■ ' i ■ ■ 32.40 32.60 32.80 33.00 33.20 |________________________ 207 ,,... ।.... ।.,.. ।..., ।....!... . ।. i,, ।,.,. ।, i . m/z 39.95 17.90% mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #65147: Azulene 128 N — AAM VAA1 5000 * i • ■ ■ • 1 1■i'1'■i■■■ ■ 1' ■ 1 32.40 32.60 32.80 33.00 33.20 I 51 102 m/z 129.15 15.53%

n/z-> 30 +747 | 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #65151: Naphthalene 128 wblfi- t 1n/,t/1/1/T/1/1/t1/E/1/3/B//-/0/1.1 .ss 32,40 32.60 32.80 33.00 33.20 — 5000 m/z 51.05 15.35? A 51 64 75 87 102 .. ..mide. n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #5168:1H-lndene 1-methylene- 128 32.40 32.60 32.80 33.00 33.20 m/ z 63.05 15.18

5000

51 63 „ 102 . m/z--> -17 4 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 T T 32.40 32.60 32.80 33.00 33.20

2710.D HP020502.M Sat Feb 09 02:31:25 2002 Page 5

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