SB1524 volatile analysis results, sample AE01938, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB04\01942F.D Vial: 14 Acq On : 4 Feb 2002 7:52 pm Operator: 201-wb Sample : nyc fb Inst : GC/MS Ins Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Hydrogen azide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

15.57 0.04 ug/L 33323 1,4-DIFLUOROBENZENE 15.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 2 2 Isobutane 58 C4H10 000075-28-5 1 3 Cyclobutylamine 71 C4H9N 002516-34-9 1 4 Propane 44 C3H8 000074-98-6 1

A Abundance Scan 670 (15.565 min): 01942F.D (-) 100.00% 43

5000 A HA 40 20000 15.20 15.40 15.60 15.80 16.00 • r ■ ■ ■ i ‘ ‘ i''' ■ i ‘' i ■ ■ ■ ■ i'''' i ‘‘' i ■ "" 41.05 24.08% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #33: Hydrogen azide 43

5000 15 15.20 15.40 15.60 15.80 16.00 29 m/ z 39.95 20.49%

mz-> Abundance 5 1111 ■ ■ i-ri 1111 10 15 ■ i ■ ■ ■ ■ i' 20 25 —mm 30 35 40 45 50 #62334: Isobutane +1PmmmWUIUTITIUUTT

43 55 60 65 70 75 80 N N V nW

15.20 15.40 15.60 15.80 16.00 5000 m/z38.95 17.65% 27 39 15 ■"■•I j ■ 11 > ।' ।' 11 ■■ 57 i ■ ■ ■ ■ i ■ ' 11 " ' I " " 11 11 ■ ■ ■ ■ i ■ ■ ■ ■ i ■11 ■ i ■ • ■ • i ■ • ■ ■ i ■ ■ ■' i ■' ■ ■ i ■

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #244: Cyclobutylamine 43 15.20 15.40 15.60 15.80 16.00 m/z43.95 4.95% 5000

27 30 39 56 72 1PTPPICTT 11TT ’ 11111117111111111111117111111177 TI 1T n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 15.20 15.40 15.60 15.80 16.00

01942F.D HP013102.M Tue Feb 05 09:50:31 2002 Page 2

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