VOC analysis results, sample AE02089, Feb 7 2002

NYC 9/11 Public Portal Document

Library Search Compound Report -msifin

Data File C:\HPCHEM\1\DATA\0 2 FEB06\2092.D Vial: 5 Acq On 6 Feb 2002 7:24 pm Operator: 201-wb Sample nyc Inst : GC/MS Ins— Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP013102.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Propane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. -aatu

15.53 0.05 ug/L 48595 1,4-DIFLUOROBENZENE 15.11 se

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propane 44 C3H8 000074-98-6 2 2 Hydrogen azide 43 HN3 007782-79-8 1 3 Cyclobutylamine 71 C4H9N 002516-34-9 1 == 4 1-Butanamine, 2-methyl- 87 C5H13N 000096-15-1 1 Abundance Scan 669 (15.531 min): 2092.D (-) m/z 43.05 100.00% 43

5000 D i r ■ ■ ■ I 15.20 15.40 15.60 15.80 40 ‘ I' •' ‘ I'' ‘ ‘ I " ' ‘ I'''11 •' " I ‘" I " ' ‘ I' m/z 41.05 18.53% n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 Abundance #38: Propane 29 N

5000 15.20 15.40 15.60 15.80

VAMAN 39 44 m/z 39.95 13.62% 15 26 ■ l ■' ■ ‘I' " 11" 19 1‘111111111111111111111111911117711TT 1‘I""I l""l" n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 •MM

Abundance #33: Hydrogen azide 43 ' ■ I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ ' I 15.20 15,40 15.60 15.80 5000 15 m/z 39.05 12.46%

/z-> Abundance ■ i ‘ 5 ■ i ‘ ■ 10 15 ‘ i11 ■ ■ i ■ 20 25 29

I30r-..,35. 40p4 45 50 55 60 65 70 75 80 11'1111 ■ ■ ■ ■ I'1 ■ ■ i ■ ■ ■ ■ i ■ ■ ‘' i' • ■ ■ i “ ■ ■ i ■

#244: Cyclobutylamine 43 AT-r-p-r-r-r-r —PPTAT 15.20 15.40 15.60 15.80 m/z 44.00 7.65%

5000

27 30 39 56 72 ■ I " " I "'1111" I" " I'1" I " " I " 1111 11 ■ “ ' i11 ■ ■ i'" ■ i ■ “ ' i' “' i1" ■ i " ' ■ 11 n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 15.20 15.40 15.60 15.80 '

2092.D HP013102.M Wed Feb 06 21:19:29 2002 Page 1

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