VOC analysis results, sample AE03015, Feb 15 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02FEB15\02719.D Vial: 9 Acq On : 15 Feb 2002 3:05 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Pentane, 2-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 19.10 0.07 ug/L 45405 CHLOROBENZENE-D5 21.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Pentane, 2-methyl- 86 C6H14 000107-83-5 4 2 (Aminomethyl)cyclopropane 71 C4H9N 002516-47-4 3 3 Hydrogen azide 43 HN3 007782-79-8 2 4 Cyanic acid, ethyl ester 71 C3H5NO 000627-48-5 2 Abundance Scan 874 (19.099 min): 02719.D (-) m/z 43.05 100.00% 43

5000 71 • • i ■ •> ■ • i ■' ■ ■ i ■ ■ ■ ■ i ■1' ■ i 39 18.80 19.00 19.20 19.40 T’EBE1""OBO—OOOTOOAITTAT ‘ICOTIEEEI—EOOI"EA"I"TTTI "‘ A‘AA‘LNAS‘AAL‘ L m/z 71.05 31.40% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #733: Pentane, 2-methyl- 43 IW 5000 T T 18.80 19.00 19.20 19.40 27 71 m/z 41.05 / 29.77% 39 15 57

m/z-> +53. mmmmmmm TTj-n-rTp-rr T 86 TH 5 10 15 20 25 3035404550556065 70 75 808590 Abundance #249: (Aminomethyl)cyclopropane 43 30 ...................... ........ ... 18.80 19.00 19.20 19.40 5000 m/z 39.95 21.04%

71 54

m/z-> mmmmmmmk 34 38 nh Nyansyanlanopanapumn *pugT 5 10 15 20253035404550556065 70 75 808590 Abundance #33: Hydrogen azide 48 18.80 19.00 19.20 19.40 m/z 39.05 18.36% N A 5000 15

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i ■ ■“i ■ ■1 trnperngrru 11) T-r-p-m-p- • » I • • • > | m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 18.80 19.00 19.20 19.40

02719.D HP021702.M Mon Feb 25 12:55:41 2002 Page 5

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