SB1524 volatile analysis results, sample AEO1636, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\02JAN28\1636.D Vial: 3 Acq On : 28 Jan 2002 6:12 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : January 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L

Peak Number 1 cis-Bicyclo[4.2.0]octa-3,7-die Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. •5.62 2.31 ug/L 1322730 1,4-DIFLUOROBENZENE 15.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual l cis-Bicyclo[4.2.0]octa-3,7-diene 106 C8H10 103148-59-0 53 2 Bicyclo[2.2.0]hex-2-ene, 5,6-dibrom 236 C6H6Br2 016622-67-6 53 3 7-Thiabicyclo[2.2.l]hept-5-ene-2,3- 182 C8H6O3S 064566-32-1 46 4 Pyridine, 4-methoxy-3-nitro- 154 C6H6N203l 031872-62-5 38 Abundance .Scan 96 (5.620 mtn): 1636.D (-) m/z 78.00 100.00% 45 78

5000 63 99 115 4 m/z-> Abundance• 40 Butt 60 80 100 120 140 160 180 200 220 240 260 280 300 73 #2024: cis-Bicyclo[4.2.0]octa-3,7-diene 275 5.20 5.40 5.60 5.80 6.00 m/z 45.10 92.91%

5000 5.20 5.40 5.60 5.80 6.00 51 m/z 49.10 74.26%

m/z-> Abundance• <40 LI i ■ ■" i ‘ “i■ ‘ i ■■■ ■ i" 60 80 100 120 140 160 180 200 220 240 260 280 300 i"111'11'irri111“11

#30926: Bicyclo[2.2.0]hex-2-ene, 5,6-dibromo-, (1.alpha.,4. ...................................... 78 5.20 5.40 5.60 5.80 6.00 5000 m/z 51.10 60.60% 51

156 238 114" ‘111 /z-> 40 60 80 100 120 140 160 180 200 220 24o'260 280 3Qo' Abundance #18218:7-Thiabicyclo[2.2.1]hept-5-ene-2,3-dlcarboxyllc anh 78 5.20 5.40 5.60 5.80 6.00 m/z 79.95 53.44%

5000

45 110 182 Www/ A I l r i 137______________________________________ 1 P " 11 'I ’ I’’’’I’’’’I’*’’IIIIIIUIIOOID—IUIIBUIABB’AA+1-5 i ■ ■ ■ ■ i ■ ■11 i ■ ' ■ i ■ ■ ■ ■ i ■ ■ m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 5.20 5.40 5.60 5.80 6.00

1636.D HP021702.M Tue Feb 19 16:34:21 2002 Page 1

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