SB1524 volatile analysis results, sample AEO1636, Jan 2002

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Data File : C:\HPCHEM\1\DATA\02JAN28\1636.D Vial: 3 Acq On : 28 Jan 2002 6:12 pm Operator: 201-wb Sample : nyc Inst : GC/MS Ins Mise : January 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 Piperazine, 3-butyl-2,5-dimeth Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 15.82 0.10 ug/L 57283 1,4-DIFLUOROBENZENE 15.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Piperazine, 3-butyl-2,5-dimethyl- 170 C10H22N2! 054410-93-4 83 2 Urea, ethyl- 88 C3H8N20 000625-52-5 83 3 Piperazine, 1,4-dimethyl- 114 C6H14N2 000106-58-1 83 4 Pentanoic acid, ethyl ester 130 C7H14O2 ______ 000539-82-2 74 Abundance Scan 684 (15.817 min): 1636.D (-) m/z 114.10 100.00%l 1 4

5000

AMAAAk— 35 50 63 II 88

m/z-> -n-p-r 20 AuuMiLL 40 13T 60 80 100 120 140 160 180 200 220 130 161 _L ■ ■ i ■ ■ ■ ■ i' ****4441** 220 15.4015.6015.8016.0016.20 m/z 35.20 43.49%

Abundance #15284: Piperazine, 3-butyl-2,5-dimethyl- 1 4 58 44 70 5000 15.40 15.60 15.80 16.00 16.20 30 84 98 m/z 49.80 38.31

m/z-> * ■ 11 • • • > ) 20 40 60 i ’ l 80 LU 100 120 140 160 ,170 .................... 180 200 220 Abundance #789: Urea, ethyl- 30 44

73 " I' ■'' I ■' 88 15.40 15.60 15.80 16.00 16.20 5000 m/z 63.10 37.97

n/z-> V J. ■ ‘ I ■ ‘ ‘ ' 11 20 40 M 100 120 140 160 180 200 '226 56

60 80 Abundance #2952: Piperazine, 1,4-dimethyl- 43 1 4 15.4015.60 15.80 16.00 16.20

Al m/z 58.30 28.31%

5000 71

56

tt/z~> 4 • i ’ * • • I* 20 40 18 9 1''1' 1 • ■' ■ i ■ ■'' i' '' ■ 1 ■'' ■ i'' ■ • i • ■ ■ ■ i ■ ■' ■ i ■ ■ 60 80 100 120 140 160 180 200 220

1636.D HP013102.M Wed Feb 20 12:29:44 2002 Page 1

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