VOC analysis results, sample AE03015, Feb 15 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\02FEB15\03250F.D Vial: 33 Acq On : 16 Feb 2002 11:11 am Operator: 201-wb Sample : nyc fb Inst : GC/MS Ins Mise : February 15, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Method : C:\HPCHEM\1\METHODS\HP021302.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Library : C:\DATABASE\NBS75K.L Peak Number 1 2,3-Dioxabicyclo[2.2.2]octane Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 15.81 0.04 ug/L 35575 1,4-DIFLUOROBENZENE 15.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2,3-Dioxabicyclo [2.2.2]octane 114 C6H10O2 000000-00-0 4 2 1-(Propenylthio)prop-l-ene 114 C6H10S 000000-00-0 3 3 1,4-Butanediamine 88 C4H12N2 000110-60-1 3 4 2,4-Imidazolidinedione, 3-methyl- 114 C4H6N202 006843-45-4 3 Abundance Scan 684 (15.809 min): 03250F.D (-) m/z 114.05 100.00% 1 4

5000

63 88 15.40 15.60 15.80 16.00 16.20

m/z-> 50 ...1......... ■ i ■ ' ■ ■ i ■ ■ ■ ' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ' ■ i 20 30 40 50 60 70 801 90 100 110 120 m/z 63.05 27.10%

Abundance #2867:2,3-Dioxabicyclo[2.2.2]octane 29

5000 81 T-rp-r-n-p-r 57 114 11'11111 15.40 15.60 15.80 16.00 16.20 44 m/z 88.00 23.90% 67

m/z-> 20 ■ i ■ ■ 30 440 H 50 60 1... 1 . 120 70 80 90 100 110 Abundance #2940: 1-(Propenylthio)prop-1-ene 1 4 41 99 p-T-n-p-r *‘1****I* 15.40 15.60 15.80 16.00 16.20 5000 m/z 49.95 12.16% N 59 73 85 ............. ............... Ill...... 1..... ■ i ■ ■ ■ ■ i ' 1 1 ■ i ■ ■ • ■ i ■ ■ ■■i■•■■i11■■ i ■ ■ ■ ■ i ' ' 1*1** m/z-> 2030405060 70 8090 100 110 120 Abundance #828:1,4-Butanediamine 30 15.40 15.60 15.80 16.00 16.20

5000 43

59

m/z—> Mm— 70 ■ i ■ ■ 20 30 40 50 60 70 80 90 100 110 120 88

03250F.D HP021302.M Mon Feb 18 15:35:30 2002 Page 1

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