SB1524 volatile analysis results, sample AEO1636, Jan 2002

NYC 9/11 Public Portal Document yuantltatlon Keport (NOC Reviewed)

Data File : C:\HPCHEM\1\DATA\02JAN28\0128R40.D Vial: 8 Acq On : 28 Jan 2002 3:52 pm Operator: 201-wb Sample : ref 40 Inst : GC/MS Ins Mise : January 28, 2002 Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Time: Jan 28 16:36 2002 Quant Results File: HP010702.RES Quant Method : C:\HPCHEM\1\METHODS\HP010702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Mon Jan 28 16:35:43 2002 Response via : Initial Calibration DataAcq Meth : HP010702

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.12 114 1109960 5.00 ug/L -0.05 2 4) CHLOROBENZENE-D5 21.79 117 996145 5.00 ug/L -0.05 52) 1,4-DICHLOROBENZENE -D4 26.97 152 496624 5.00 ug/L -0.05

System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 727784 5.05 ug/L -0.07 Spiked Amount 5.000 Recovery = 101.00% 3) 4-BROMOFLUOROBENZENE 24.37 174 409568 5.45 ug/L -0.05 Spiked Amount 5.000 Recovery = 109.00% 25) TOLUENE-D8 18.48 98 1300297 4.90 ug/L -0.05 Spiked Amount 5.000 Recovery = 98.00% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.87 85 2712928 /4055. 77 99 5) CHLOROMETHANE 5.51 50 1908871 9% 35.33 ug/L 97 6) VINYL CHLORIDE 5.58 62 2301217 51.57 ug/L 100 7) BROMOMETHANE 6.62 94 1602198 45.41 ug/L 99 8) CHLOROETHANE 6.72 64 1214556 38.86 ug/L < of ) 97 9) TRICHLOROFLUOROMETHANE 7.29 101 4243410 48.17 ug/L 98 11) 1,1,2-Trichloro-1,2,2-trif 8.19 101 13779 0.24 ug/L 76 12) ACETONE 8.27 43 375477 26.09 ug/L 93 13) 1,1-DICHLOROETHENE 8.60 61 3263297 37.00 ug/L 99 14) METHYLENE CHLORIDE 9.63 49 3187285 31.20 ug/L 96 15) METHYL TERT BUTYL ETHER 9.93 73 2859044 47.92 ug/L 93 16) TRANS-1,2-DICHLOROETHENE 10.29 61 3257566 37.29 ug/L 94 17) 1,1-DICHLOROETHANE 11.18 63 3493635 36.42 ug/L 97 18) 2-BUTANONE (MEK) 12.02 43 712879 38.66 ug/L 96 19) 2,2-DICHLOROPROPANE 12.40 77 3080082 45.87 ug/L 98 20) CIS-1,2-DICHLOROETHENE 12.51 96 1942976 39.89 ug/L 90 21) CHLOROFORM 12.84 83 4207448 38.36 ug/L 98 22) BROMOCHLOROMETHANE 13.22 49 1951894 35.26 ug/L 92 23) 1,2-DICHLOROETHANE 14.56 62 3616518 39.70 ug/L 98 26) 1,1,1-TRICHLOROETHANE 13.73 97 3907365 43.02 ug/L 95 27) 1,1-DICHLOROPROPENE 14.06 75 3059578 43.47 ug/L 98 28) CARBON TETRACHLORIDE 14.32 117 3843613 42.10 ug/L 98 29) BENZENE 14.65 78 6735692 36.89 ug/L 97 30) TRICHLOROETHENE 15.94 95 2300318 41.08 ug/L 96 31) 1,2-DICHLOROPROPANE 16.29 63 1930238 36.81 ug/L 97 32) DIBROMOMETHANE 16.97 174 964801 41.63 ug/L 88 33) BROMODICHLOROMETHANE 16.81 83 3219102 41.52 ug/L 99 34) 2-CHLOROETHYL VINYL ETHER 17.28 63 714882 43.36 ug/L 94 (#) = qualifier out of range (m) = manual integration 0128R40.D HP010702.M Thu Feb 14 09:29:13 2002 Page 1

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