GCMS calibration table, sample AD31129, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN0902\31129A.D Vial: 26 Acq On : 10 Jan 2002 3:31 pm Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.46 2.58 ug/1 755205 1,4-Dichlorobenzene-d4 11.52

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 1,3-Dioxolane, 2-pentadecyl - 284 C18H36O2_ 004360-57-0 9 Abundance Scan 264 (7,465 min): 31129A.D (-) m/ z ” 72. 95 100.00% 73

5000 43 7.20 N 7.60 7.40 1 IUTr । i । i । 7.80 3? 1, | 50 55, , 67, । ,1 ■ ■ i ■ 87 103 T 1 I I I I ] I t I 1 I 1 ! ' I' | I ! * 1 11 r’t’ ! J I * "pr 1 1***l4***1*I m/z 43.00 32.54% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73 i t i i | | > ri । / — i i

5000 7.20 7.40 7.60 7.80 55 m/z 45.05 12.67% 45 87 27 | 39, : ‘LB TfIBBBnI.n 1 ■ ' i 1 ■ ■ ■ i ■ ■ ■ ■ i ' • ' ■ i ' 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #6203 Slane tatramethgi 73

7.20 7.40 7.60 7.80 5000 m/z 41.05 11.66% 45 15 53 59 88 m/z-> 10 20 30 40 50 60 70 80 90 100___ 110 Abundance #1793: Pentane, 3-methoxy- ' 73 7.20 7.40 7.60 7.80 m/z 71.00 6.68% 5000 45

27 33 39 ■ • i ■ 1 • ' I 1 1 1 1 I 1 1 1 1 I1 55 1 1 ‘ * ,rJ 1 TTI— । • i ■ ■ ‘ ■ i ■ ■ ■ ■ i ■ ‘ ■ i ' 1 11 J j [ i 11 [ r j "i I rt i । pt m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31129A.D GCMS0103.M Wed Feb 06 09:21:22 2002 Page 1

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