GCMS analysis results for sample AD29286, Jan 22 2002

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Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\JANO 302\29286.D Vial: 29 Acq On 4 Jan 2002 1:48 pm Operator: 209 GALOS Sample gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 7.47 4.20 ug/ 879777 1,4-Dichlorobenzene-d4 11.52

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Silane,/tetramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Ditolane, 2-methyl- 88 C4H802 000497-26-7 9 4 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 264 (7.466 min): 29286.D (-) m/z 73.00 100.00% 73

5000 43

87 7.20 7.40 7.60 7.80 38 |, 1 50 55. 60 67, । 103 ■ ' i 1 ‘ ■ I 1 • ■ 1 I ' IITTTT I । ‘ I ■ I m/z 43.05 32.62% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 . . । , 7Tl | > . . . 7.20 7.40 ' 7.60 7.80 55 m/z 45.05; 12.08% 27 45 87 ,1, 1 39, * I • ■ i 11 i ■ ■ I TT ............ 1 * * I ‘ I.......... . ,, ‘ 1 * 1 • * I * • T-r-j-n miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73 ■ I ' ‘ ‘ ' I 1 ‘ 1 ‘ 1 4* Is I i . . I 7.20 7.40 7.60 7.80 5000 rn/z 41.05 11.42% 45 j 15 TIIPPTT 5359 .. ... 88 m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane, 2-methyl- 'm I [I ri TI"l 1 I | rsfi | I I i l 73 7.20 7.40 7.60 7.80 m/z 71.0.0 7.00% 5000 43 58 27 87 i , ' l • • • • I ■ ■ ‘ i 1 — i1- ■ i ■ ■ H • ■ 1 ■ i ■ 1 ■ ■ i ■ • ■ ■ i ■ ■ ■ ■ i ■ ■ ■ • i • 1 TmumgfTTTLTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

29286.D GCMS0103.M Fri Jan 11 08:29:41 2002 Page 1

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