NYC 9/11 Public Portal Document yucuLltdtlon Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN2502\30936A.D Vial: 3
Acq On 2 : 25 Jan 2002 11:09 am Operator: 209 GALOS
Sample 1 : REINJECT Inst : GC/MS 209
Mise : I Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Jan 25 12:11 2002 Quant Results File: GCMS1126.RES
A Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
1 Title . * : 209 625/TCLP calibration table
Last Update : Tue Jan 22 11:56:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0103
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Internal Standards R.T. Qlon Response Cone Units Dev (Min)
------ v------------------
1) 1,4-Dichlorobenzene-d4 11.48 152 911232 20.00 ug/1 -0.22
10) Naphthalene-d8 15.08 136 3542840 20.00 ug/1 -0.23
17) Acenaphthene-diO 20.35 164 1714317 20.00 ug/1 -0.23
2 9) Phenanthrene-dl0 24.75 188 2491314 20.00 ug/1 -0.24
38) Chrysene-dl2 32.79 240 1584825 20.00 ug/1 -0.25
44) Perylene-dl2 36.84 264 1035076 20.00 ug/1 -0.27
System Monitoring Compounds
37) 2,4-DDD 29.83 235 152044 5.55 ug/mL -0.24
Spiked Amount 5.000 Recovery = 111.00%
f
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.31 74 107 N.D.
3) bis(2-Chloroethyl)ether 10.95 93 1343 N.D.
4) 1,3-Dichlorobenzene 11.41 146 1146 N.D.
5)1,4 -Dichlorobenzene 11.53 146 1506 N.D.
6)1,2-Dichlorobenzene 12.05 146 1109 N.D.
7) 2,2’ -oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) 'Hexachloroethane 12.87 117 228 N.D.
11) Nitrobenzene 13.20 77 605 N.D.
12) 1sophorone 13.86 82 2618 N.D.
13) bis(2-Chloroethoxy)methane 14.52 93 1548 N.D.
14) 1,2,4-Trichlorobenzene 14.99 180 1099 N.D.
15). Naphthalene 15.13 128 4441 N.D.
16) Hexachlorobutadiene 15.69 225 468 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.64 162 1918 N.D.
20) Dimethylphthalate 19.75 163 2558 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 19.89 152 2308 N.D.
23) Acenaphthene 20.44 153 2500 N.D.
24) 2,4-Dinitrotoluene 20.81 165 1465 N.D.
25) Dithylphthalate 21.87 149 3849 N.D.
26) 4-Chlorophenyl-phenylether 22.00 204 795 N.D.
27) Flurene 21.95 166 2321 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
------- - -------- -- -----------
(#) = qualifier outof range (m) = manual integration
30936A.D GCMS1126.M Fri Jan 25 12:13:12 2002 Page 1
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NYC-WTC_000018777
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