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GCMS analysis results, sample AD30936, January 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AD30936 conducted on 1/28/2002, measuring organic compounds including surrogates and unknown compounds.

NYC-WTC_000018775–000018794

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C: \HPCHEM\ 1 \DATA\ JAN2 502\30936A.D Vial: 3 Acq On : 25 Jan 2002 11:09 am Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 12:11 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update • : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.39 168 522 N.D. 31) 4-Bromophenyl-phenylether 23.46 248 456 N.D. 32) Hexachlorobenzene 23.87 284 485 N.D. 3 3) Phenanthrene 24.82 178 5017 N.D. 3 4) Anthracene 24.96 178 2453 N.D. 35) Di-n-butylphthalate 26.78 149 13590 N.D. 3 6) Fluoranthene 28.44 202 2885 N.D. 39) Pyrene 29.10 202 3293 N.D. 40) Butylbenzylphthalate 31.28 149 1749 N.D. 41) Benzo(a)anthracene 32.86 228 8031 N.D. 42) Bis(2-ethylhexyl)phthalate 33.09 149 14147 N.D. 43) Chrysene 32.86 228 8031 N.D. 45) Di-n-Octylphthalate 34.82 149 2153 N.D. 46) Benzo(b)fluoranthene 35.88 252 8087 N.D. 47) Benzo(k)fluoranthene 35.88 252 8087 N.D. 4 8) Benzo(a)pyrene 36.68 252 2315 N.D. 49) Indeno(l,2,3-cd)pyrene 40.44 276 371 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 41.50 276 647 N.D.

(#) = qualifier out of range (m) = manual integration 30936A.D GCMS1126.M Fri Jan 25 12:13:15 2002 Page 2

NYC-WTC_000018778

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NYC-WTC_000018778Source: NYC Law Department, mirrored locally

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