NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\JAN2502\30649.D Vial: 34
Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS
Sample : REINJECT Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Jan 28 8:25 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Jan 25 15:57:52 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0103
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.48 152 2257653 20.00 ug/1 -0.22
10) Naphthalene-d8 15.09 136 8487805 20.00 ug/1 -0.22
17) Acenaphthene-diO 20.35 164 4106555 20.00 ug/1 -0.23
29) Phenanthrene-diO 24.77 188 5734113 20.00 ug/1 -0.23
38) Chrysene-dl2 32.80 240 3442233 20.00 ug/1 -0.23
44) Perylene-dl2 36.86 264 2107498 20.00 ug/1 -0.26
System Monitoring Compounds
37) 2,4-DDD 29.83 235 254417 4.04 ug/mL -0.24
Spiked Amount 5.000 Recovery = 80.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.13 74 776 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 13.13 117 103 N.D.
11) Nitrobenzene 12.85 77 278 N.D.
12) Isophorone 14.12 82 178 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.15 128 4175 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 18.16 162 626 N.D.
20) Dimethylphthalate 20.08 163 2669 N.D.
21) 2,6-Dinitrotoluene 19.92 165 356 N.D.
22) Acenaphthylene 20.01 152 1308 N.D.
23) Acenaphthene 20.37 153 170 N.D.
24) 2,4-Dinitrotoluene 21.16 165 322 N.D.
25) Diethylphthalate 21.87 149 2359 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30649.D GCMS1126.M Mon Jan 28 08:28:06 2002 Page 1
NYC-WTC_000004249
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