GCMS analysis summary, sample AD27392, Dec 2001

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\JANI502\2 7392.D Vial: 9 Acq On : 15 Jan 2002 6:46 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 4 14:01 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS0103

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.50 152 838111 20.00 ug/1 -0.20 10) ’Naphthalene-d8 15.10 136 3268854 20.00 ug/1 -0.21 17) Acenaphthene-diO 20.36 164 1675388 20.00 ug/1 -0.22 29) Phenanthrene-diO 24.78 188 2272505 20.00 ug/1 -0.22 38) Chrysene-dl2 32.80 240 1453627 20.00 ug/1 -0.24 44) Perylene-dl2 36.87 264 1031716 20.00 ug/1 -0.25

System Monitoring Compounds 37) 2,4-DDD 29.85 235 144032 5.76 ug/mL -0.22 Spiked Amount 5.000 Recovery = 115.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.16 128 2281 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 20.82 165 175 N.D. 25) Diethylphthalate 21.88 149 1024 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 27392.D GCMS1126.M Mon Feb 04 14:02:45 2002 Page 1

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