NYC-WTC_000017931
Laboratory report documenting GCMS analysis of sample AD30472 conducted on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 10 pages
GC/MS analysis results for sample AD30905, Jan 28 2002
Machine-extracted title · confidence 100%Laboratory report documenting gas chromatography mass spectrometry results for sample AD30905 conducted on January 28, 2002.
NYC-WTC_000018640–000018649Folder label: “GCMS X 12/19/01 A 1/2/02”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\DEC3101\30905.D Vial: 45 Acq On 2 Jan 2002 7:33 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 9:50 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update •: Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. QIon Response Cone Units Dev(Min)
1) l,4-Dichlorobenzene-d4 11.67 152 908417 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 3479935 20.00 ug/1 -0.02 17) Acenaphthene-dlO 20.56 164 1782357 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 2567457m 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1531266m 20.00 ug/1 -0.01 44) Perylene-dl2 37.11 264 842865m 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.06 235 148765 5.27 ug/mL 0.00 Spiked Amount 5.000 Recovery = 105.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.22 74 1114 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. s 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.35 77 528 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 975 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.25 165 194 N.D. 25) Diethylphthalate 22.16 149 1553 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 30905.D GCMS1126.M Fri Jan 25 09:51:20 2002 Page 1
NYC-WTC_000018642
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NYC-WTC_000018642Source: NYC Law Department, mirrored locally
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