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GC/MS analysis results for sample AD30904, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.

NYC-WTC_000018624–000018639

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\30904.D Vial: 44 Acq On 2 Jan 2002 6:35 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 9:48 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 752466 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 2881514 20.00 ug/1 -0.03 17) Acenaphthene-dlO 20.56 164 1434259 20.00 ug/1 -0.02 2 9) Phenanthrene-dl0 24.98 188 2085328 20.00 ug/1 -0.01 38) Chrysene-dl2 33.02 240 1180884 20.00 ug/1 -0.01 44) Perylene-dl2 37.13 264 632755 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 115829 5.05 ug/mL 0.00 Spiked Amount 5.000 Recovery = 101.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.20 74 1285 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.32 128 277 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachiorocyc1opentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.28 163 204 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.40 165 171 N.D. 25) Diethylphthalate 22.17 149 1165 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 22.82 77 102 N.D.

(#) = qualifier out of range (m) = manual integration 30904.D GCMS1126.M Fri Jan 25 09:48:21 2002 Page 1

NYC-WTC_000018626

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NYC-WTC_000018626Source: NYC Law Department, mirrored locally

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