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GCMS analysis results for sample AD30473, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30473 conducted on January 24, 2002.

NYC-WTC_000017969–000017979

Folder label: “GCMS X 12/14/01 A 12/31/01

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Scanned page image, NYC-WTC_000017974
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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File : C:\HPCHEM\l\DATA\DEC3101\30473.D Vial: 14 Acq On : 31 Dec 2001 11:37 pm Operator: 209 GALOS Sample : gems scan 12/14fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.609 275 279 309 rBV 325215 1093212 15.72% 3.219% 2 11.676 717 722 740 rBV 1889735 4941290 71.06% 14.548% 3 15.275 1109 1114 1135 rBV 2348754 6307103 90.70% 18.570% 4 20.563 1683 1690 1727 rBV 2594670 6954089 100.00% 20.475% 5 24.988 2165 2172 2206 rBV2 1909069 6445572 92.69% 18.978%

6 30.064 2719 2725 2741 rBV 345168 839442 12.07% 2.472% 7 33.020 3041 3047 3074 rBV2 1462153 4584641 65.93% 13.498% 8 37.124 3486 3494 3518 rBV 703414 2798917 40.25% 8.241%

Sum of corrected areas: 33964266

30473.D GCMS1126.M Wed Jan 16 08:24:32 2002

NYC-WTC_0000 17974

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NYC-WTC_000017974Source: NYC Law Department, mirrored locally

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