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GCMS analysis results for sample AD30483, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30483 conducted on January 24, 2002.

NYC-WTC_000017949–000017957

Folder label: “GCMS X 12/14/01 A 12/31/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\l\DATA\DEC3101\30483.D Vial: 13 Acq On : 31 Dec 2001 10:39 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.612 276 280 293 rBV 363266 1013116 14.12% 2.888% 2 11.669 718 722 758 rBV 1835985 5213023 72.63% 14.858% 3 15.277 1110 1115 1135 rBV 2501990 6506281 90.65% 18.544% 4 20.556 1684 1690 1716 rBV 2658676 7177530 100.00% 20.457% 5 24.981 2166 2172 2210 rBV2 2041823 6707596 93.45% 19.118%

6 30.067 2720 2726 2741 rBV 384656 906909 12.64% 2.585% 7 33.023 3041 3048 3074 rBV2 1546565 4551897 63.42% 12.974% 8 37.117 3486 3494 3532 rBV2 769574 3009646 41.93% 8.578%

Sum of corrected areas: 35085998 30483.D GCMS1126.M Wed Jan 16 08:25:24 2002

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NYC-WTC_000017954

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NYC-WTC_000017954Source: NYC Law Department, mirrored locally

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