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GCMS analysis results for sample AD30472, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30472 conducted on January 24, 2002.

NYC-WTC_000017931–000017939

Folder label: “GCMS X 12/14/01 A 12/31/01

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NYC 9/11 Public Portal Document LSC Area Percent Report

. Data File : C:\HPCHEM\1\DATA\DEC3101\30472.D Vial: 7 Acq On : 31 Dec 2001 4:48 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF• Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.608 275 279 310 rBV 357231 1173824 15.76% 3.124% 2 11.675 717 722 758 rBV 2113007 5576364 74.88% 14.843% 3 15.283 1109 1115 1135 rBV 2625811 6874784 92.31% 18.298% 4 20.562 1684 1690 1716 rBV 2866193 7447172 100.00% 19.822% 5 24.987 2165 2172 2205 rBV 2349692 7163265 96.19% 19.066%

6 30.063 2719 27252735 rBV 415205 927651 12.46% 2.469% 7 33.019 3040 3047 3067 rBV2 1684981 5066444 68.03% 13.485% 8 37.123 3486 3494 3521 rBV2 899629 3340710 44.86% 8.892% % Sum of corrected areas: 37570214

30472.D GCMS1126.M Wed Jan 16 08:23:35 2002

NYC-WTC_000017936

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NYC-WTC_000017936Source: NYC Law Department, mirrored locally

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