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GCMS analysis results for sample AD30490, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30490 conducted on January 24, 2002.

NYC-WTC_000017913–000017921

Folder label: “GCMS X 12/14/01 A 12/31/01

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Scanned page image, NYC-WTC_000017918
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NYC 9/11 Public Portal Document LSC Area Percent Report

• Data File : C:\HPCHEM\1\DATA\DEC3101\30490.D Vial: 12 Acq On : 31 Dec 2001 9:40 pm Operator: 209 GALOS Sample : gems scan 12/14fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF. Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.612 276 280 309 rBV 386465 1122504 15.14% 3.073% 2 11.670 718 722 761 rBV 2094339 5415429 73.05% 14.827% 3 15.278 1110 1115 1135 rBV 2714210 6773510 91.37% 18.545% 4 20.557 1684 1690 1717 rBV 2796186 7412954 100.00% 20.296% 5 24.981 2166 2172 2217 rBV2 2122205 7025687 94.78% 19.235%

6 30.067 2720 2726 2737 rBV 402526 923621 12.46% 2.529% 7 33.023 3042 3048 3075 rBV2 1647326 4855006 65.49% 13.292% 8 37.118 3487 3494 3522 rBV2 771325 2996062 40.42% 8.203%

Sum of corrected areas: 36524773

30490.D GCMS1126.M Wed Jan 16 08:27:55 2002

NYC-WTC_000017918

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NYC-WTC_000017918Source: NYC Law Department, mirrored locally

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