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GCMS analysis results for sample AD30471, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30471 conducted on January 24, 2002.

NYC-WTC_000017922–000017930

Folder label: “GCMS X 12/14/01 A 12/31/01

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Scanned page image, NYC-WTC_000017927
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\DEC3101\30471.D Vial: 10 Acq On : 31 Dec 2001 7:44 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 • MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209.625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.613 276 280 315 rBV 370644 1146454 16.06% 3.251% 2 11.670 717 722 753 rBV 1902765 5252406 73.59% 14.892% 3 15.278 1109 1115 1136 rBV 2533916 6533021 91.53% 18.523% 4 20.557 1684 1690 1717 rBV 2635803 7137629 100.00% 20.238% 5 24.982 2166 2172 2209 rBV2 2068317 6740170 94.43% 19.111%

6 30.068 2720 2726 2737 rBV 354743 821187 11.51% 2.328% 7 33.024 3041 3048 3073 rBV2 1582541 4675783 65.51% 13.257% 8 37.118 3487 3494 3525 rBV 787340 2962615 41.51% 8.400%

Sum of corrected areas: 35269265

30471.D GCMS1126.M Wed Jan 16 08:22:55 2002

NYC-WTC_000017927

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NYC-WTC_000017927Source: NYC Law Department, mirrored locally

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