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GCMS analysis results for sample AD30352, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.

NYC-WTC_000017808–000017832

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2 701\30352.D Vial: 19 Acq On : 28 Dec 2001 5:38 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 12:15 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.05 178 3771 N.D. 34) Anthracene 25.18 178 808 N.D. 35) Di-n-butylphthalate 27.01 149 93901 0.46 ug/1 # 3 6) Fluoranthene 28.75 202 2092 N.D. 3 9) Pyrene 29.42 202 2024 N.D. 40) Butylbenzylphthalate 31.53 149 313 N.D. 41) Benzo(a)anthracene 33.02 228 6531 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 7564 N.D. 43) Chrysene 33.02 228 6531 N.D. 45) Di-n-Octylphthalate 35.06 149 206 N.D. 46) Benzo(b)fluoranthene 0.00 252 . 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. ‘ 48) Benzo(a)pyrene 37.12 252 4473 N.D. 49) Indeno (1,2,3-cd) pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30352.D GCMS1126.M Mon Dec 31 12:18:00 2001 Page 2

NYC-WTC_0000 17811

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NYC-WTC_000017811Source: NYC Law Department, mirrored locally

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