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GCMS analysis results for sample AD30425, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.

NYC-WTC_000017703–000017723

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2 701\30425.D Vial: 5 Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 27 15:53 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title ’: 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 3 2) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.04 178 721 N.D. 34) Anthracene 25.04 178 721 N.D. 35) Di-n-butylphthalate 27.01 149 73763 0.37 ug/1 # 99 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 4 0) Butylbenzylphthalate 31.51 149 248 N.D. 41) Benzo(a)anthracene 33.02 228 4447 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 10287 N.D. 43) Chrysene 33.10 228 393 N.D. 45) Di-n-Octylphthalate 35.10 149 836 N.D. 46) Benzo(b)fluoranthene 36.12 252 1213 N.D. 47) Benzo(k)fluoranthene 36.12 252 463 N.D. ' 4 8) Benzo(a)pyrene 37.12 252 4778 N.D. 4 9) Indeno(1,2,3 -cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30425.D GCMS1126.M Mon Dec 31 12:38:57 2001 Page 2

NYC-WTC_000017706

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NYC-WTC_000017706Source: NYC Law Department, mirrored locally

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