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GCMS analysis results for sample AD30356, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30356 conducted on January 10, 2002.

NYC-WTC_000017770–000017781

Folder label: “GCMS X 12/13/01 A 12/27/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC2701\30356.D Vial: 21 Acq On : 28 Dec 2001 7:34 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 12:16 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title .: 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.04 178 704 N.D. 3 4) Anthracene 25.04 178 704 N.D. 35) Di-n-butylphthalate 27.01 149 84467 0.40 ug/1 # 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.02 228 4959 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 6465 N.D. 43) Chrysene 33.02 228 4959 N.D. 45) Di-n-Octylphthalate 35.46 149 112 N.D. 4 6) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.12 252 4549 N.D. 49) Indeno (1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30356.D GCMS1126.M Mon Dec 31 12:17:06 2001 Page 2

NYC-WTC_0000 17773

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NYC-WTC_000017773Source: NYC Law Department, mirrored locally

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